benzyl 3,4-methano-3,4-dideoxy-β-L-arabinopyranoside

Base Information

Chemical Name:benzyl 3,4-methano-3,4-dideoxy-β-L-arabinopyranoside
CAS No.:124044-03-7
Molecular Formula:C₂₅H₃₀N₂O₆
Molecular Weight:454.523
Hs Code.:

benzyl 3,4-<exo-N-(N-benzyloxycarbonyl-L-alanyl)aminomethyl>methano-3,4-dideoxy-β-L-arabinopyranoside

Synonyms:

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Chemical Property of benzyl 3,4-methano-3,4-dideoxy-β-L-arabinopyranoside

Chemical Property:

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Technology Process of benzyl 3,4-methano-3,4-dideoxy-β-L-arabinopyranoside

There total 4 articles about benzyl 3,4-methano-3,4-dideoxy-β-L-arabinopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 3401-36-3
2-Benzyloxycarbonylamino-propionic acid 2,5-dioxo-pyrrolidin-1-yl ester

: 124044-01-5
benzyl 3,4-(exo-aminomethyl)methano-3,4-dideoxy-β-L-arabinopyranoside

: 124044-03-7
benzyl 3,4-methano-3,4-dideoxy-β-L-arabinopyranoside

Guidance literature:: In dichloromethane; for 72h; Ambient temperature;

Reference yield:

: 120408-67-5
benzyl 3,4-(exo-cyano)methano-3,4-dideoxy-β-L-arabinopyranoside

: 124044-03-7
benzyl 3,4-methano-3,4-dideoxy-β-L-arabinopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / LiAlH₄ / diethyl ether / 0.5 h / 0 °C

2: 84 percent / CH₂Cl₂ / 72 h / Ambient temperature

With lithium aluminium tetrahydride; In diethyl ether; dichloromethane;

Reference yield:

: 1142-20-7
N-benzyloxycarbonyl-L-alanine

: 124044-03-7
benzyl 3,4-methano-3,4-dideoxy-β-L-arabinopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 35 percent / DCC / dioxane / 24 h / Ambient temperature

2: 84 percent / CH₂Cl₂ / 72 h / Ambient temperature

With dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane;