trans-[RuH(CN)(PPh₂(CH₂)2PPh₂)2]

Base Information

Chemical Name:trans-[RuH(CN)(PPh₂(CH₂)2PPh₂)2]
CAS No.:210572-48-8
Molecular Formula:C₅₃H₄₉NP₄Ru
Molecular Weight:924.944
Hs Code.:

trans-[RuH(CN)(PPh<sub>2</sub>(CH<sub>2</sub>)2PPh<sub>2</sub>)2]

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Chemical Property of trans-[RuH(CN)(PPh₂(CH₂)2PPh₂)2]

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Technology Process of trans-[RuH(CN)(PPh₂(CH₂)2PPh₂)2]

There total 2 articles about trans-[RuH(CN)(PPh₂(CH₂)2PPh₂)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: potassium cyanide

: trans-[RuH(η2-H2)(PPh2(CH2)2PPh2)2]BPh4

: 210572-48-8
trans-[RuH(CN)(PPh₂(CH₂)2PPh₂)2]

Guidance literature:: In methanol; byproducts: H2; trans-Ru-contg. compd. (0.37 mmol) was suspd. in MeOH and KCN (0.61 mmol) added with stirring; the mixt. was stirred overnight under Ar; filtered off, washed with MeOH and dried in vac.; purifn. by dissolving in toluene and filtering off the salt; evapn. of the solvent; elem. anal.;
DOI:10.1039/b0056871

Reference yield:

: potassium cyanide

: 356528-26-2,357261-87-1
Ru((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2H(FHF)

: 210572-48-8
trans-[RuH(CN)(PPh₂(CH₂)2PPh₂)2]

Guidance literature:: DOI:10.1039/b101007g

Reference yield: 86.0%

: 67969-82-8
tetrafluoroboric acid diethyl ether

: 210572-48-8
trans-[RuH(CN)(PPh₂(CH₂)2PPh₂)2]

: 319905-26-5
trans-[RuH(CNBF₃)(PPh₂(CH₂)2PPh₂)2]

: trans-[Ru(BF₄)(CN)(PPh₂(CH₂)2PPh₂)2]

: [Ru(H₂)(CNBF₃)(PPh₂(CH₂)2PPh₂)2]FHF

Guidance literature:: In benzene; HBF4*Et2O (0.07 mmol) was added to a soln. of trans-Ru-contg. compd. (0.05 mmol) in benzene; stirring for 30 min under Ar; filtered off, washed with benzene and dried in vac.; slow evapn. of a concd. soln. in CH2Cl2; elem. anal.;
DOI:10.1039/b0056871