Technology Process of C28H38O4
There total 5 articles about C28H38O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
phenyl(2,4,6-trihydroxy-3,5-diisopentylphenyl)methanone;
With
sodium hydride;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 0.0833333h;
Inert atmosphere;
4-iodo-2-methyl-but-1-ene;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/jo500027k
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: aluminum (III) chloride / nitrobenzene / 0.5 h / 20 °C / Inert atmosphere
1.2: 2 h / 65 °C / Inert atmosphere
2.1: potassium hydroxide / water / 1.33 h / 0 °C / Inert atmosphere
3.1: palladium on activated charcoal; hydrogen / ethanol / 2 h / 20 °C
4.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 20 °C / Inert atmosphere
4.2: 1 h / 20 °C / Inert atmosphere
With
aluminum (III) chloride; palladium on activated charcoal; hydrogen; sodium hydride; potassium hydroxide;
In
ethanol; water; nitrobenzene; N,N-dimethyl-formamide;
DOI:10.1021/jo500027k
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium hydroxide / water / 1.33 h / 0 °C / Inert atmosphere
2.1: palladium on activated charcoal; hydrogen / ethanol / 2 h / 20 °C
3.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 20 °C / Inert atmosphere
3.2: 1 h / 20 °C / Inert atmosphere
With
palladium on activated charcoal; hydrogen; sodium hydride; potassium hydroxide;
In
ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo500027k
