Technology Process of 2-diphenylmethyl-1-methyl-1,2-diazetidin-3-one
There total 7 articles about 2-diphenylmethyl-1-methyl-1,2-diazetidin-3-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 94 percent / acetic acid / ethanol / 24 h / Heating
2: 100 percent / K2CO3 / acetone / 24 h / Heating
3: 91 percent / NaBH3CN, aq. HCl / tetrahydrofuran; methanol
4: 54 percent / triethylamine / benzene / 12 h / Ambient temperature
5: 87 percent / trifluoroacetic acid / CH2Cl2 / 48 h / Ambient temperature
6: 63 percent / triethylamine, toluene-p-sulphonyl azide / CH2Cl2 / Ambient temperature
7: 1.) H2O / 1.) diethyl ether, 4.5 h, irradiated; 2.) benzene, 4 h, reflux
With
hydrogenchloride; 4-toluenesulfonyl azide; water; sodium cyanoborohydride; potassium carbonate; acetic acid; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; acetone; benzene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 100 percent / K2CO3 / acetone / 24 h / Heating
2: 91 percent / NaBH3CN, aq. HCl / tetrahydrofuran; methanol
3: 54 percent / triethylamine / benzene / 12 h / Ambient temperature
4: 87 percent / trifluoroacetic acid / CH2Cl2 / 48 h / Ambient temperature
5: 63 percent / triethylamine, toluene-p-sulphonyl azide / CH2Cl2 / Ambient temperature
6: 1.) H2O / 1.) diethyl ether, 4.5 h, irradiated; 2.) benzene, 4 h, reflux
With
hydrogenchloride; 4-toluenesulfonyl azide; water; sodium cyanoborohydride; potassium carbonate; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane; acetone; benzene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 91 percent / NaBH3CN, aq. HCl / tetrahydrofuran; methanol
2: 54 percent / triethylamine / benzene / 12 h / Ambient temperature
3: 87 percent / trifluoroacetic acid / CH2Cl2 / 48 h / Ambient temperature
4: 63 percent / triethylamine, toluene-p-sulphonyl azide / CH2Cl2 / Ambient temperature
5: 1.) H2O / 1.) diethyl ether, 4.5 h, irradiated; 2.) benzene, 4 h, reflux
With
hydrogenchloride; 4-toluenesulfonyl azide; water; sodium cyanoborohydride; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane; benzene;