2,6-diethoxyphenyldimethylphosphaneborane

Base Information

• Chemical Name: 2,6-diethoxyphenyldimethylphosphaneborane
• CAS No.: 125325-31-7
• Molecular Formula: C₁₂H₂₂BO₂P
• Molecular Weight: 240.09
• Mol file: 125325-31-7.mol

Synonyms:

Chemical Property of 2,6-diethoxyphenyldimethylphosphaneborane

Chemical Property:

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Technology Process of 2,6-diethoxyphenyldimethylphosphaneborane

There total 1 articles about 2,6-diethoxyphenyldimethylphosphaneborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

chlorodimethylphosphine-borane (54220-72-3) + 2,4-diethoxybenzene (2049-73-2) → 2,6-diethoxyphenyldimethylphosphaneborane (125325-31-7)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; diethyl ether; hexane; byproducts: LiCl; under Ar or N, dropwise addn. of dimethylchlorophosphaneborane in THF tomixt. of 1,3-diethoxybenzene in diethyl ether and n-butyllithium in hexane; filtration, evapn. under vac., recrystn. from abs. ethanol, elem. anal.,purity greater 95 percent;

DOI:10.1016/0022-328X(89)87163-3

upstream raw materials:

chlorodimethylphosphine-borane

2,4-diethoxybenzene