4,10b-dihydro-4-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl][2]benzogermino[2,1-d]-1,2,3,4-trithiagermole

Base Information

• Chemical Name: 4,10b-dihydro-4-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl][2]benzogermino[2,1-d]-1,2,3,4-trithiagermole
• CAS No.: 476303-86-3
• Molecular Formula: C₃₆H₆₆GeS₃Si₆
• Molecular Weight: 836.221

Synonyms:

Chemical Property of 4,10b-dihydro-4-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl][2]benzogermino[2,1-d]-1,2,3,4-trithiagermole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,10b-dihydro-4-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl][2]benzogermino[2,1-d]-1,2,3,4-trithiagermole

There total 10 articles about 4,10b-dihydro-4-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl][2]benzogermino[2,1-d]-1,2,3,4-trithiagermole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-2-germanaphthalene (392335-69-2) + sulfur (7704-34-9) → 4,10b-dihydro-4-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl][2]benzogermino[2,1-d]-1,2,3,4-trithiagermole (476303-86-3)

Guidance literature:

In benzene; under Ar, soln. was stirred for 48 h at room temp.; solvent was evapd., residue was chromd.; elem. anal.;

DOI:10.1021/om020879m

Reference yield: 55.0%

sulfur (10544-50-0) + 2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-2-germanaphthalene (392335-69-2) → 4,10b-dihydro-4-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl][2]benzogermino[2,1-d]-1,2,3,4-trithiagermole (476303-86-3)

Guidance literature:

In benzene; Ge compd. reacted with excess of S8 at room temp., stirred for 48 jh; solvent removed, chromy., elem. anal.;

DOI:10.1246/cl.2002.818

Reference yield: 35.0%

2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-2-germanaphthalene (392335-69-2) + cis-2,3-diphenylthiirane → 4,10b-dihydro-4-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl][2]benzogermino[2,1-d]-1,2,3,4-trithiagermole (476303-86-3)

Guidance literature:

In tetrahydrofuran; under Ar, soln. was stirred for 5 h at room temp.; solvent was evapd., residue was chromd.; elem. anal.;

DOI:10.1021/om020879m

upstream raw materials:

2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-2-germanaphthalene

sulfur

sulfur

2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-1,2-dihydro-2-germanaphthalene

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 476303-86-3 4,10b-dihydro-4-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl][2]benzogermino[2,1-d]-1,2,3,4-trithiagermole

Send

Send

Metric Ton KG G Pound L ML

Send

Send