9,10-Dimethoxy-2-mesitylimino-4-(2,4-dimethylanilino)-6,7-dihydro-2H-triazino(2,1-a)isoquinoline hydriodide

Base Information

Chemical Name:9,10-Dimethoxy-2-mesitylimino-4-(2,4-dimethylanilino)-6,7-dihydro-2H-triazino(2,1-a)isoquinoline hydriodide
CAS No.:85686-83-5
Molecular Formula:C₃₀H₃₃N₅O₂*HI
Molecular Weight:623.537
Hs Code.:

Synonyms:

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Chemical Property of 9,10-Dimethoxy-2-mesitylimino-4-(2,4-dimethylanilino)-6,7-dihydro-2H-triazino(2,1-a)isoquinoline hydriodide

Chemical Property:

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Technology Process of 9,10-Dimethoxy-2-mesitylimino-4-(2,4-dimethylanilino)-6,7-dihydro-2H-triazino(2,1-a)isoquinoline hydriodide

There total 9 articles about 9,10-Dimethoxy-2-mesitylimino-4-(2,4-dimethylanilino)-6,7-dihydro-2H-triazino(2,1-a)isoquinoline hydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 85686-92-6
4-ethylthio-9,10-dimethoxy-2-mesitylimino-6,7-dihydro-2H-1,3,5-triazino<2,1-a>isoquinoline hydroiodide

: 95-68-1
2,4-Xylidine

: 85686-83-5
9,10-Dimethoxy-2-mesitylimino-4-(2,4-dimethylanilino)-6,7-dihydro-2H-triazino(2,1-a)isoquinoline hydriodide

Guidance literature:

Reference yield:

: 24456-59-5
6,7-dimethoxy-3,4-dihydroisoquinoline-1(2H)-thione

: 85686-83-5
9,10-Dimethoxy-2-mesitylimino-4-(2,4-dimethylanilino)-6,7-dihydro-2H-triazino(2,1-a)isoquinoline hydriodide

Guidance literature:: Multi-step reaction with 8 steps

2: 80 percent / NH₃ / ethanol / 4 h / Heating

3: 79 percent / sodium hydride / benzene / 16 h / Heating

4: POCl₃ / 2 h / Heating

5: CHCl₃ / 20 h / Heating

6: 80 percent / Lawesson's reagent / dioxane / 16 h / 95 - 100 °C

7: 80 percent / tetrahydrofuran / 2 h / Heating

8: 66 percent

With Lawessons reagent; ammonia; sodium hydride; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; ethanol; chloroform; benzene;

Reference yield:

: 85686-51-7
9,10-dimethoxy-3,4,6,7-tetrahydro-2H-1,3,5-triazino<2,1-a>isoquinolin-2,4-dione

: 85686-83-5
9,10-Dimethoxy-2-mesitylimino-4-(2,4-dimethylanilino)-6,7-dihydro-2H-triazino(2,1-a)isoquinoline hydriodide

Guidance literature:: Multi-step reaction with 5 steps

1: POCl₃ / 2 h / Heating

2: CHCl₃ / 20 h / Heating

3: 80 percent / Lawesson's reagent / dioxane / 16 h / 95 - 100 °C

4: 80 percent / tetrahydrofuran / 2 h / Heating

5: 66 percent

With Lawessons reagent; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; chloroform;