Technology Process of C58H70O10Si
There total 3 articles about C58H70O10Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Methyltriphenylphosphonium bromide;
With
potassium tert-butylate;
In
tetrahydrofuran;
at 0 ℃;
for 0.5h;
C57H68O11Si;
In
tetrahydrofuran;
at 0 ℃;
for 0.5h;
DOI:10.1021/np100729d
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / -30 - 0 °C
2.1: methyllithium / tetrahydrofuran; diethyl ether / -78 - 20 °C
2.2: Inert atmosphere
3.1: triethyl borane; tri-n-butyl-tin hydride / tetrahydrofuran; toluene / 5 h / -40 - -15 °C / in air
4.1: pyridine; trifluoroacetic anhydride / acetonitrile / 7 h / 0 °C
5.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C
5.2: 0.5 h / 0 °C
With
pyridine; triethyl borane; potassium tert-butylate; tetrabutyl ammonium fluoride; methyllithium; tri-n-butyl-tin hydride; trifluoroacetic anhydride;
In
tetrahydrofuran; diethyl ether; toluene; acetonitrile;
4.1: Pummerer reaction / 4.2: Pummerer reaction / 5.1: Wittig reaction / 5.2: Wittig reaction;
DOI:10.1021/np100729d
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: pyridine; trifluoroacetic anhydride / acetonitrile / 7 h / 0 °C
2.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C
2.2: 0.5 h / 0 °C
With
pyridine; potassium tert-butylate; trifluoroacetic anhydride;
In
tetrahydrofuran; acetonitrile;
1.1: Pummerer reaction / 1.2: Pummerer reaction / 2.1: Wittig reaction / 2.2: Wittig reaction;
DOI:10.1021/np100729d
