C₄₄H₆₇N₃O₁₃

Base Information

Chemical Name:C₄₄H₆₇N₃O₁₃
CAS No.:1235514-52-9
Molecular Formula:C₄₄H₆₇N₃O₁₃
Molecular Weight:846.028
Hs Code.:

C<sub>44</sub>H<sub>67</sub>N<sub>3</sub>O<sub>13</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₄H₆₇N₃O₁₃

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Technology Process of C₄₄H₆₇N₃O₁₃

There total 3 articles about C₄₄H₆₇N₃O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 1235514-66-5
Boc-Aoac-Phe-OEt

: 61257-02-1
5-O-mycaminosyl tylonolide

: 1235514-52-9
C₄₄H₆₇N₃O₁₃

Guidance literature:: Boc-Aoac-Phe-OEt; With trifluoroacetic acid; at 20 ℃; for 1h;

5-O-mycaminosyl tylonolide; In dimethyl sulfoxide; at 50 ℃; for 12h; pH=4.7; sodium acetate buffer;
DOI:10.1134/S1068162010020159

Reference yield:

: 3081-24-1
H-Phe-OEt

: 1235514-52-9
C₄₄H₆₇N₃O₁₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 1 h / 0 °C

1.2: 4 h / 20 °C

2.1: trifluoroacetic acid / 1 h / 20 °C

2.2: 12 h / 50 °C / pH 4.7 / sodium acetate buffer

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1134/S1068162010020159