Technology Process of C23H29F8NO2S2
There total 3 articles about C23H29F8NO2S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: BuLi / tetrahydrofuran / -70 °C
1.2: 78 percent / I2 / tetrahydrofuran / -40 °C
2.1: 56 percent / 1-methyl-pyrrolidin-2-one / 18 h / 120 - 150 °C
3.1: 28 percent / MCPBA / CH2Cl2 / 72 h / 20 °C
4.1: 16 percent / triflic anhydride / CH2Cl2 / 18 h / 20 °C
With
n-butyllithium; trifluoromethylsulfonic anhydride; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; 1-methyl-pyrrolidin-2-one; dichloromethane;
DOI:10.1002/ejoc.200400702
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 56 percent / 1-methyl-pyrrolidin-2-one / 18 h / 120 - 150 °C
2: 28 percent / MCPBA / CH2Cl2 / 72 h / 20 °C
3: 16 percent / triflic anhydride / CH2Cl2 / 18 h / 20 °C
With
trifluoromethylsulfonic anhydride; 3-chloro-benzenecarboperoxoic acid;
In
1-methyl-pyrrolidin-2-one; dichloromethane;
DOI:10.1002/ejoc.200400702
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 28 percent / MCPBA / CH2Cl2 / 72 h / 20 °C
2: 16 percent / triflic anhydride / CH2Cl2 / 18 h / 20 °C
With
trifluoromethylsulfonic anhydride; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
DOI:10.1002/ejoc.200400702
