4-(3,5-difluoro-4-trifluoromethylsulfanyl-phenyl)-4'-propyl-bicyclohexyl

Base Information

Chemical Name:4-(3,5-difluoro-4-trifluoromethylsulfanyl-phenyl)-4'-propyl-bicyclohexyl
CAS No.:851341-10-1
Molecular Formula:C₂₂H₂₉F₅S
Molecular Weight:420.53
Hs Code.:

Synonyms:4-(3,5-difluoro-4-trifluoromethylsulfanyl-phenyl)-4'-propyl-bicyclohexyl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(3,5-difluoro-4-trifluoromethylsulfanyl-phenyl)-4'-propyl-bicyclohexyl

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Technology Process of 4-(3,5-difluoro-4-trifluoromethylsulfanyl-phenyl)-4'-propyl-bicyclohexyl

There total 2 articles about 4-(3,5-difluoro-4-trifluoromethylsulfanyl-phenyl)-4'-propyl-bicyclohexyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 3872-23-9
Copper(I) trifluoromethanethiolate

: 140918-34-9
4-(3,5-difluoro-4-iodo-phenyl)-4'-propyl-bicyclohexyl

: 851341-10-1
4-(3,5-difluoro-4-trifluoromethylsulfanyl-phenyl)-4'-propyl-bicyclohexyl

Guidance literature:: In 1-methyl-pyrrolidin-2-one; at 120 - 150 ℃; for 18h;
DOI:10.1002/ejoc.200400702

Reference yield:

: 138074-21-2
2,6-difluoro-4-(trans-4-(trans-4-propylcyclohexyl)cyclohexyl)benzene

: 851341-10-1
4-(3,5-difluoro-4-trifluoromethylsulfanyl-phenyl)-4'-propyl-bicyclohexyl

Guidance literature:: Multi-step reaction with 2 steps

1.1: BuLi / tetrahydrofuran / -70 °C

1.2: 78 percent / I₂ / tetrahydrofuran / -40 °C

2.1: 56 percent / 1-methyl-pyrrolidin-2-one / 18 h / 120 - 150 °C

With n-butyllithium; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one;
DOI:10.1002/ejoc.200400702