Technology Process of C46H42N2O6*C34H34N2O6
There total 5 articles about C46H42N2O6*C34H34N2O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 80 percent
2: 98 percent / pyridinium chloride / 200 °C
3: 53 percent / Cs2CO3 / dimethylformamide / 60 °C
4: 1.) Cu(CH3CN)4(1+)*BF4(1-), Cs2CO3; 2.) KCN / 1.) CH2Cl2; 2.) CH3CN, H2O, r.t., several days
With
potassium cyanide; tetrakis(acetonitrile)copper(I)tetrafluoroborate; pyridine hydrochloride; caesium carbonate;
In
N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)84501-3
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 80 percent
2: 98 percent / pyridinium chloride / 200 °C
3: 53 percent / Cs2CO3 / dimethylformamide / 60 °C
4: 1.) Cu(CH3CN)4(1+)*BF4(1-), Cs2CO3; 2.) KCN / 1.) CH2Cl2; 2.) CH3CN, H2O, r.t., several days
With
potassium cyanide; tetrakis(acetonitrile)copper(I)tetrafluoroborate; pyridine hydrochloride; caesium carbonate;
In
N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)84501-3
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 53 percent / Cs2CO3 / dimethylformamide / 60 °C
2: 1.) Cu(CH3CN)4(1+)*BF4(1-), Cs2CO3; 2.) KCN / 1.) CH2Cl2; 2.) CH3CN, H2O, r.t., several days
With
potassium cyanide; tetrakis(acetonitrile)copper(I)tetrafluoroborate; caesium carbonate;
In
N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)84501-3
