3-thiobenzoylmethyl-4,5,6-triphenylpyridazine

Base Information

Chemical Name:3-thiobenzoylmethyl-4,5,6-triphenylpyridazine
CAS No.:132575-74-7
Molecular Formula:C₃₀H₂₂N₂S
Molecular Weight:442.584
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-thiobenzoylmethyl-4,5,6-triphenylpyridazine

Chemical Property:

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Technology Process of 3-thiobenzoylmethyl-4,5,6-triphenylpyridazine

There total 5 articles about 3-thiobenzoylmethyl-4,5,6-triphenylpyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 132575-73-6
3-benzoylmethyl-4,5,6-triphenylpyridazine

: 132575-74-7
3-thiobenzoylmethyl-4,5,6-triphenylpyridazine

Guidance literature:: With diphosphorus pentasulfide; In xylene; for 2h; Heating;

Reference yield:

: 31590-01-9
4,5,6-triphenyl-3(2H)-pyridazinone

: 132575-74-7
3-thiobenzoylmethyl-4,5,6-triphenylpyridazine

Guidance literature:: Multi-step reaction with 4 steps

1: 55.5 percent / phosphorus pentasulfide / pyridine / 4 h / Heating

2: 62 percent / sodium ethoxide / ethanol / 2 h / Heating

3: 55 percent / pyridine / 0.5 h / Heating

4: 45 percent / phosphorus pentasulfide / xylene / 2 h / Heating

With pyridine; diphosphorus pentasulfide; sodium ethanolate; In pyridine; ethanol; xylene;

Reference yield:

: 132575-64-5
3-chloro-4,5,6-triphenylpyridazine

: 132575-74-7
3-thiobenzoylmethyl-4,5,6-triphenylpyridazine

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) thiourea, 2.) 2.5 M sodium hydroxide / 1.) absolute ethanol, 20 deg C, 3 h, 2.) 1 h, reflux

2: 62 percent / sodium ethoxide / ethanol / 2 h / Heating

3: 55 percent / pyridine / 0.5 h / Heating

4: 45 percent / phosphorus pentasulfide / xylene / 2 h / Heating

With pyridine; diphosphorus pentasulfide; sodium hydroxide; sodium ethanolate; thiourea; In ethanol; xylene;