IrH₂(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄

Base Information

Chemical Name:IrH₂(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄
CAS No.:752245-70-8
Molecular Formula:C₃₈H₅₇F₆IrO₂P₂
Molecular Weight:914.027
Hs Code.:

IrH<sub>2</sub>(C<sub>6</sub>H<sub>2</sub>(CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>(OP(C(CH<sub>3</sub>)3)2)2)C<sub>8</sub>H<sub>14</sub>

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Chemical Property of IrH₂(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄

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Technology Process of IrH₂(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄

There total 4 articles about IrH₂(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 931-88-4,931-87-3,25267-51-0
cis-Cyclooctene

: 686274-20-4
[p-(3,5-CF₃)2C₆H₃C₆H₂-2,6-(OP(tBu)2)2]IrH₂

: 752245-69-5
Ir(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄

: 752245-70-8,752250-85-4
IrH₂(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄

: 752245-70-8,752250-85-4
IrH₂(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄

Guidance literature:: In further solvent(s); soln. of Ir-complex in methylcyclohexane-d14 was cooled to -125°C, soln. of cyclooctene in methylcyclohexane-d14 was added, mixed at -110°C, shimmed, heated at -70°C; monitored by NMR;
DOI:10.1021/ja048393f

Reference yield:

: 931-88-4,931-87-3,25267-51-0
cis-Cyclooctene

: 686274-20-4
[p-(3,5-CF₃)2C₆H₃C₆H₂-2,6-(OP(tBu)2)2]IrH₂

: 752245-69-5
Ir(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄

: 752245-70-8,752250-85-4
IrH₂(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄

: 752245-70-8,752250-85-4
IrH₂(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄

Guidance literature:: In further solvent(s); soln. of Ir-complex in methylcyclohexane-d14 was cooled to -125°C, soln. of cyclooctene in methylcyclohexane-d14 was added, mixed at -110°C, shimmed, heated at -70°C; monitored by NMR;
DOI:10.1021/ja048393f

Reference yield:

: 931-88-4,931-87-3,25267-51-0
cis-Cyclooctene

: 686274-20-4
[p-(3,5-CF₃)2C₆H₃C₆H₂-2,6-(OP(tBu)2)2]IrH₂

: 2037-26-5
⁽²⁾H₈-toluene

: 752245-70-8,752250-85-4
IrH₂(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄

: 752245-70-8,752250-85-4
IrH₂(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₈H₁₄

: Ir⁽³⁺⁾*⁽²⁾H^(1-)*C₆⁽²⁾H₄C⁽²⁾H₃^(1-)*C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2^(1-)=Ir⁽²⁾H(C₆H₂(CF₃)2C₆H₃(OP(C(CH₃)3)2)2)C₆⁽²⁾H₄C⁽²⁾H₃

Guidance literature:: In ⁽²⁾H₈-toluene; Ir-complex in toluene-d8 was cooled to -110°C, soln. of cyclooctene in toluene-d8 was added, shimmed to -90°C, 3 h;
DOI:10.1021/ja048393f