Technology Process of C28H34O2Si
There total 5 articles about C28H34O2Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
[2,2]bipyridinyl; silver hexafluoroantimonate; palladium dichloride;
In
methanol; water;
at 60 ℃;
Inert atmosphere;
DOI:10.1002/chem.201200694
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrahydrofuran; diethyl ether / 1 h / 0 °C
2: [2,2]bipyridinyl; silver hexafluoroantimonate; palladium dichloride / methanol; water / 60 °C / Inert atmosphere
With
[2,2]bipyridinyl; silver hexafluoroantimonate; palladium dichloride;
In
tetrahydrofuran; methanol; diethyl ether; water;
DOI:10.1002/chem.201200694
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: acetic anhydride; pyridinium chlorochromate / dichloromethane / 1 h / 20 °C / Molecular sieve
2.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C
2.2: 12 h / 20 °C
3.1: isopropylmagnesium chloride / tetrahydrofuran / 1.5 h / 0 - 20 °C
4.1: tetrahydrofuran; diethyl ether / 1 h / 0 °C
5.1: [2,2]bipyridinyl; silver hexafluoroantimonate; palladium dichloride / methanol; water / 60 °C / Inert atmosphere
With
[2,2]bipyridinyl; silver hexafluoroantimonate; isopropylmagnesium chloride; acetic anhydride; sodium hydride; pyridinium chlorochromate; palladium dichloride;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; water;
DOI:10.1002/chem.201200694