Technology Process of C28H34O2Si
There total 5 articles about C28H34O2Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
[2,2]bipyridinyl; silver hexafluoroantimonate; palladium dichloride;
In
methanol; water;
at 60 ℃;
Inert atmosphere;
DOI:10.1002/chem.201200694
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrahydrofuran; diethyl ether / 1 h / 0 °C
2: [2,2]bipyridinyl; silver hexafluoroantimonate; palladium dichloride / methanol; water / 60 °C / Inert atmosphere
With
[2,2]bipyridinyl; silver hexafluoroantimonate; palladium dichloride;
In
tetrahydrofuran; methanol; diethyl ether; water;
DOI:10.1002/chem.201200694
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: acetic anhydride; pyridinium chlorochromate / dichloromethane / 1 h / 20 °C / Molecular sieve
2.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C
2.2: 12 h / 20 °C
3.1: isopropylmagnesium chloride / tetrahydrofuran / 1.5 h / 0 - 20 °C
4.1: tetrahydrofuran; diethyl ether / 1 h / 0 °C
5.1: [2,2]bipyridinyl; silver hexafluoroantimonate; palladium dichloride / methanol; water / 60 °C / Inert atmosphere
With
[2,2]bipyridinyl; silver hexafluoroantimonate; isopropylmagnesium chloride; acetic anhydride; sodium hydride; pyridinium chlorochromate; palladium dichloride;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; water;
DOI:10.1002/chem.201200694
