Methyl 3-methoxy-4-methyl-2-nitrobenzoate

Base Information

• Chemical Name: Methyl 3-methoxy-4-methyl-2-nitrobenzoate
• CAS No.: 128450-32-8
• Molecular Formula: C10H11NO5
• Molecular Weight: 225.201
• Hs Code.: 2918990090
• Mol file: 128450-32-8.mol

Synonyms:benzoic acid, 3-methoxy-4-methyl-2-nitro-, methyl ester;Methyl 3-methoxy-4-methyl-2-nitrobenzoate;LogP

Chemical Property of Methyl 3-methoxy-4-methyl-2-nitrobenzoate

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Refractive Index: 1.537
• Boiling Point: 343.188 °C at 760 mmHg
• Flash Point: 154.531 °C
• PSA: 81.35000
• Density: 1.255 g/cm³
• LogP: 2.22160

Purity/Quality:

99% ^*data from raw suppliers

Methyl3-methoxy-4-methyl-2-nitrobenzoate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 3-methoxy-4-methyl-2-nitrobenzoate

There total 1 articles about Methyl 3-methoxy-4-methyl-2-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.7%

3-hydroxy-4-methyl-2-nitro-benzoic acid (6946-15-2) + methyl iodide (74-88-4) → methyl 3-methoxy-4-methyl-2-nitrobenzoate (128450-32-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield: 93.8%

methyl 3-methoxy-4-methyl-2-nitrobenzoate (128450-32-8) → 2-amino-3-methoxy-4-methyl-benzoic acid methyl ester (5544-24-1)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; at 20 ℃; under 2585.81 Torr;

upstream raw materials:

3-hydroxy-4-methyl-2-nitro-benzoic acid

methyl iodide

Downstream raw materials:

2-amino-3-methoxy-4-methyl-benzoic acid methyl ester

Refernces