(3-fluorobenzyltriphenylphosphinium)bis(maleonitriledithiolate)nickelate

Base Information

Chemical Name:(3-fluorobenzyltriphenylphosphinium)bis(maleonitriledithiolate)nickelate
CAS No.:1253931-23-5
Molecular Formula:C₈N₄NiS₄*C₂₅H₂₁FP
Molecular Weight:710.483
Hs Code.:

Synonyms:

Suppliers and Price of (3-fluorobenzyltriphenylphosphinium)bis(maleonitriledithiolate)nickelate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (3-fluorobenzyltriphenylphosphinium)bis(maleonitriledithiolate)nickelate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3-fluorobenzyltriphenylphosphinium)bis(maleonitriledithiolate)nickelate

There total 1 articles about (3-fluorobenzyltriphenylphosphinium)bis(maleonitriledithiolate)nickelate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: nickel(II) chloride hexahydrate

: 89302-81-8
(3-fluorobenzyl)(triphenyl)phosphonium bromide

: 5466-54-6
disodium cis-1,2-dicyano-1,2-ethylenedithiolate

: 1253931-23-5
(3-fluorobenzyltriphenylphosphinium)bis(maleonitriledithiolate)nickelate

Guidance literature:: With I₂; In methanol; MeOH soln. of Na-salt added to MeOH soln. of NiCl2*6H2O with stirring, stirred for 45 min at room temp., I2 in MeOH added, warmed to 45°Cfor 15 min, MeOH soln. of ligand dropped slowly, cooled after 1.5 h; filtered, washed with cold MeOH, Et2O, dried in air; elem. anal.;
DOI:10.1016/j.molstruc.2010.07.042