8,8'-Diselenodioctanoic acid

Base Information

• Chemical Name: 8,8'-Diselenodioctanoic acid
• CAS No.: 22686-32-4
• Molecular Formula: C₁₆H₃₀O₄Se₂
• Molecular Weight: 444.332
• Mol file: 22686-32-4.mol

Synonyms:

Chemical Property of 8,8'-Diselenodioctanoic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 8,8'-Diselenodioctanoic acid

There total 1 articles about 8,8'-Diselenodioctanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.6%

8-bromooctanoic acid (17696-11-6) → di-(1-carboxylheptyl) diselenide (22686-32-4)

Guidance literature:

With selenium; sodium tetrahydroborate; In tetrahydrofuran; water; at 50 ℃; Inert atmosphere;

DOI:10.1039/c9cc00252a

Reference yield:

1-Bromoheptane (629-04-9) + di-(1-carboxylheptyl) diselenide (22686-32-4) → 9-Selena-hexadecansaeure (50514-84-6)

Guidance literature:

Multistep reaction; (i) HOCH₂SO₂Na, aq. NH₃, (ii) /BRN= 1697160/, EtOH;

Reference yield:

di-(1-carboxylheptyl) diselenide (22686-32-4) + benzyl chloride (100-44-7) → 8-(Benzylseleno)caprylsaeure (43169-93-3)

Guidance literature:

Multistep reaction; (i) HOCH2SO2H , aq. NH3, (ii) /BRN= 471308/;

upstream raw materials:

8-bromooctanoic acid

Downstream raw materials:

9-Selena-hexadecansaeure

8-(Benzylseleno)caprylsaeure

8'-(4-Methylbenzylseleno)-caprylsaeure

8-(4'-Bromphenylseleno)-caprylsaeure

Refernces