2-Benzenesulfinyl-1-[(4aS,5S,11cR)-5-chloro-7-(4-methoxy-benzenesulfonyl)-2,3,4,4a,5,6,7,11c-octahydro-pyrido[3,2-c]carbazol-1-yl]-ethanone

Base Information

Chemical Name:2-Benzenesulfinyl-1-[(4aS,5S,11cR)-5-chloro-7-(4-methoxy-benzenesulfonyl)-2,3,4,4a,5,6,7,11c-octahydro-pyrido[3,2-c]carbazol-1-yl]-ethanone
CAS No.:84986-94-7
Molecular Formula:C₃₀H₂₉ClN₂O₅S₂
Molecular Weight:597.156
Hs Code.:

2-Benzenesulfinyl-1-[(4aS,5S,11cR)-5-chloro-7-(4-methoxy-benzenesulfonyl)-2,3,4,4a,5,6,7,11c-octahydro-pyrido[3,2-c]carbazol-1-yl]-ethanone

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Chemical Property of 2-Benzenesulfinyl-1-[(4aS,5S,11cR)-5-chloro-7-(4-methoxy-benzenesulfonyl)-2,3,4,4a,5,6,7,11c-octahydro-pyrido[3,2-c]carbazol-1-yl]-ethanone

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Technology Process of 2-Benzenesulfinyl-1-[(4aS,5S,11cR)-5-chloro-7-(4-methoxy-benzenesulfonyl)-2,3,4,4a,5,6,7,11c-octahydro-pyrido[3,2-c]carbazol-1-yl]-ethanone

There total 8 articles about 2-Benzenesulfinyl-1-[(4aS,5S,11cR)-5-chloro-7-(4-methoxy-benzenesulfonyl)-2,3,4,4a,5,6,7,11c-octahydro-pyrido[3,2-c]carbazol-1-yl]-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 7031-27-8
(phenylthio)acetic acid chloride

: 84960-67-8
cis-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)-sulfonyl>-1H-pyrido<3,2-c>carbazole

: 84986-94-7,89063-44-5,89063-45-6
2-Benzenesulfinyl-1-[(4aS,5S,11cR)-5-chloro-7-(4-methoxy-benzenesulfonyl)-2,3,4,4a,5,6,7,11c-octahydro-pyrido[3,2-c]carbazol-1-yl]-ethanone

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid;
DOI:10.1021/ja00345a081

Reference yield:

: 80664-26-2
N-<(4-methoxyphenyl)sulfonyl>-2-methylindole-3-carboxaldehyde

: 84986-94-7,89063-44-5,89063-45-6
2-Benzenesulfinyl-1-[(4aS,5S,11cR)-5-chloro-7-(4-methoxy-benzenesulfonyl)-2,3,4,4a,5,6,7,11c-octahydro-pyrido[3,2-c]carbazol-1-yl]-ethanone

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / 4A molecular sieves

2: 50 percent / N(i-Pr)2Et / chlorobenzene / 120 °C

3: 91 percent / Zn, AcOH / tetrahydrofuran; H₂O / 20 °C

4: 91 percent / MCPBA

With 4 A molecular sieve; acetic acid; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; zinc; In tetrahydrofuran; water; chlorobenzene;
DOI:10.1021/ja00345a081

Reference yield:

: 88981-61-7
2,2,2-trichloroethyl cis-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)sulfonyl>-1H-pyrido<3,2-c>carbazole-1-carboxylate

: 84986-94-7,89063-44-5,89063-45-6
2-Benzenesulfinyl-1-[(4aS,5S,11cR)-5-chloro-7-(4-methoxy-benzenesulfonyl)-2,3,4,4a,5,6,7,11c-octahydro-pyrido[3,2-c]carbazol-1-yl]-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / Zn, AcOH / tetrahydrofuran; H₂O / 20 °C

2: 91 percent / MCPBA

With acetic acid; 3-chloro-benzenecarboperoxoic acid; zinc; In tetrahydrofuran; water;
DOI:10.1021/ja00345a081