8,14-Dimethyl-4,6-diphenyl-4,6,8,18-tetrazatetracyclo[8.8.0.02,7.012,17]octadeca-1(10),2(7),11,13,15,17-hexaene-3,5,9-trione

Base Information

Chemical Name:8,14-Dimethyl-4,6-diphenyl-4,6,8,18-tetrazatetracyclo[8.8.0.02,7.012,17]octadeca-1(10),2(7),11,13,15,17-hexaene-3,5,9-trione
CAS No.:177082-79-0
Molecular Formula:C₂₈H₂₀N₄O₃
Molecular Weight:460.492
Hs Code.:
DSSTox Substance ID:DTXSID80382957
Wikidata:Q82174456

Synonyms:177082-79-0;8,14-Dimethyl-4,6-diphenyl-4,6,8,18-tetrazatetracyclo[8.8.0.02,7.012,17]octadeca-1(10),2(7),11,13,15,17-hexaene-3,5,9-trione;ZINC01036826;Oprea1_358858;SCHEMBL12325793;DTXSID80382957;CCG-256333

Suppliers and Price of 8,14-Dimethyl-4,6-diphenyl-4,6,8,18-tetrazatetracyclo[8.8.0.02,7.012,17]octadeca-1(10),2(7),11,13,15,17-hexaene-3,5,9-trione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 8,14-Dimethyl-4,6-diphenyl-4,6,8,18-tetrazatetracyclo[8.8.0.02,7.012,17]octadeca-1(10),2(7),11,13,15,17-hexaene-3,5,9-trione

Chemical Property:

Vapor Pressure:1.82E-18mmHg at 25°C
XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:460.15354051
Heavy Atom Count:35
Complexity:919

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC2=CC3=C(C4=C(N(C3=O)C)N(C(=O)N(C4=O)C5=CC=CC=C5)C6=CC=CC=C6)N=C2C=C1

Technology Process of 8,14-Dimethyl-4,6-diphenyl-4,6,8,18-tetrazatetracyclo[8.8.0.02,7.012,17]octadeca-1(10),2(7),11,13,15,17-hexaene-3,5,9-trione

There total 3 articles about 8,14-Dimethyl-4,6-diphenyl-4,6,8,18-tetrazatetracyclo[8.8.0.02,7.012,17]octadeca-1(10),2(7),11,13,15,17-hexaene-3,5,9-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66400-26-8
6-methylamino-1,3-diphenyl-1H-pyrimidine-2,4-dione

: 177082-79-0
5,9-Dimethyl-2,4-diphenyl-4H,5H-2,4,5,12-tetraaza-benzo[a]anthracene-1,3,6-trione

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / diphenyl ether / 2 h / 220 - 250 °C

2: 75 percent / POCl₃ / 50 - 60 °C

3: 2) 2 N aq. NaOH / 1) DMF, 60 deg C to 70 deg C, 2 h, 2) r.t., 5 h

With sodium hydroxide; trichlorophosphate; In diphenylether;
DOI:10.1002/prac.19963380129

Reference yield:

: 177082-44-9
5-hydroxy-8-methyl-1,3-diphenyl-pyrido<2,3-d>pyrimidine-2,4,7-trione

: 177082-79-0
5,9-Dimethyl-2,4-diphenyl-4H,5H-2,4,5,12-tetraaza-benzo[a]anthracene-1,3,6-trione

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / POCl₃ / 50 - 60 °C

2: 2) 2 N aq. NaOH / 1) DMF, 60 deg C to 70 deg C, 2 h, 2) r.t., 5 h

With sodium hydroxide; trichlorophosphate;
DOI:10.1002/prac.19963380129

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 177082-56-3
5-chloro-6-formyl-8-methyl-1,3-diphenyl-pyrido<2,3-d>pyrimidine-2,4,7(1H,3H,8H)-trione

: 177082-79-0
5,9-Dimethyl-2,4-diphenyl-4H,5H-2,4,5,12-tetraaza-benzo[a]anthracene-1,3,6-trione

Guidance literature:: With sodium hydroxide; Yield given. Multistep reaction; 1) DMF, 60 deg C to 70 deg C, 2 h, 2) r.t., 5 h;
DOI:10.1002/prac.19963380129