Technology Process of C26H40O6
There total 11 articles about C26H40O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran
2: acetic acid
3: pyridine / dichloromethane / -80 °C
4: pyridinium p-toluenesulfonate / dichloromethane
5: water; potassium carbonate / methanol
7: sodium hydride / tetrahydrofuran / 0 - 20 °C
8: diethyl ether / 0 °C
9: sodium cyanoborohydride; zinc(II) iodide / dichloromethane / 20 °C
With
pyridine; water; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium cyanoborohydride; potassium carbonate; acetic acid; zinc(II) iodide;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane;
6: Swern oxidation / 7: Wittig-Horner olefination;
DOI:10.1016/j.cclet.2010.11.023
- Guidance literature:
-
Multi-step reaction with 6 steps
1: pyridinium p-toluenesulfonate / dichloromethane
2: water; potassium carbonate / methanol
4: sodium hydride / tetrahydrofuran / 0 - 20 °C
5: diethyl ether / 0 °C
6: sodium cyanoborohydride; zinc(II) iodide / dichloromethane / 20 °C
With
water; pyridinium p-toluenesulfonate; sodium hydride; sodium cyanoborohydride; potassium carbonate; zinc(II) iodide;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane;
3: Swern oxidation / 4: Wittig-Horner olefination;
DOI:10.1016/j.cclet.2010.11.023