bisphosphine oxide

Base Information

Chemical Name:bisphosphine oxide
CAS No.:80953-58-8
Molecular Formula:C₂₃H₂₂F₃O₃P
Molecular Weight:434.395
Hs Code.:

<m-(trifluoromethyl)phenyl>bis<o-(methoxymethyl)phenyl>phosphine oxide

Synonyms:

Suppliers and Price of bisphosphine oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of bisphosphine oxide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of bisphosphine oxide

There total 3 articles about bisphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54057-97-5
diethyl <3-(trifluoromethyl)phenyl>phosphonate

: 80953-58-8
bisphosphine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / PCl₅ / CCl₄ / Ambient temperature

2: 1.) n-BuLi / 1.) ether, hexane, -72 deg C, 0.5 h, 2.) -72 deg C, 1 h

With n-butyllithium; phosphorus pentachloride; In tetrachloromethane;
DOI:10.1021/jo00348a013

Reference yield:

: 402-26-6
3-(trifluoromethyl)phenylmagnesium bromide

: 80953-58-8
bisphosphine oxide

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / 1.) -76 deg C, 1.5 h, 2.) RT, 1.5 h

2: 98 percent / PCl₅ / CCl₄ / Ambient temperature

3: 1.) n-BuLi / 1.) ether, hexane, -72 deg C, 0.5 h, 2.) -72 deg C, 1 h

With n-butyllithium; phosphorus pentachloride; In tetrachloromethane; diethyl ether;
DOI:10.1021/jo00348a013

Reference yield:

: 52711-30-5
1-bromo-2-(methoxymethyl)benzene

: 80953-57-7
ethyl <3-(trifluoromethyl)phenyl>phosphonochloridate

: 80953-58-8
bisphosphine oxide

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) ether, hexane, -72 deg C, 0.5 h, 2.) -72 deg C, 1 h;
DOI:10.1021/jo00348a013