acide<<(tritylamino-2 thiazolyl-4)(methoxyimino)-acetyl>amino>-7 methoxy-3 oxo-8 thia-4 aza-1 bicyclo<4.2.0> octene-2 carboxylique-2(6-R,S)(7-R,S)(Z)

Base Information

Chemical Name:acide<<(tritylamino-2 thiazolyl-4)(methoxyimino)-acetyl>amino>-7 methoxy-3 oxo-8 thia-4 aza-1 bicyclo<4.2.0> octene-2 carboxylique-2(6-R,S)(7-R,S)(Z)
CAS No.:128990-05-6
Molecular Formula:C₃₃H₂₉N₅O₆S₂
Molecular Weight:655.755
Hs Code.:

acide<<(tritylamino-2 thiazolyl-4)(methoxyimino)-acetyl>amino>-7 methoxy-3 oxo-8 thia-4 aza-1 bicyclo<4.2.0> octene-2 carboxylique-2(6-R,S)(7-R,S)(Z)

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Chemical Property of acide<<(tritylamino-2 thiazolyl-4)(methoxyimino)-acetyl>amino>-7 methoxy-3 oxo-8 thia-4 aza-1 bicyclo<4.2.0> octene-2 carboxylique-2(6-R,S)(7-R,S)(Z)

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Technology Process of acide<<(tritylamino-2 thiazolyl-4)(methoxyimino)-acetyl>amino>-7 methoxy-3 oxo-8 thia-4 aza-1 bicyclo<4.2.0> octene-2 carboxylique-2(6-R,S)(7-R,S)(Z)

There total 10 articles about acide<<(tritylamino-2 thiazolyl-4)(methoxyimino)-acetyl>amino>-7 methoxy-3 oxo-8 thia-4 aza-1 bicyclo<4.2.0> octene-2 carboxylique-2(6-R,S)(7-R,S)(Z) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102192-12-1
[(3S,4R)-3-Amino-2-oxo-4-((E)-styryl)-azetidin-1-yl]-acetic acid 4-nitro-benzyl ester

: 128990-05-6
acide<<(tritylamino-2 thiazolyl-4)(methoxyimino)-acetyl>amino>-7 methoxy-3 oxo-8 thia-4 aza-1 bicyclo<4.2.0> octene-2 carboxylique-2(6-R,S)(7-R,S)(Z)

Guidance literature:: Multi-step reaction with 9 steps

1: 63 percent / tetrahydrofuran / 1 h / Heating

2: 1.) ozone 2.) dimethyl sulfide / 1.) CH₂Cl₂, -70 deg C 2.) CH₂Cl₂, 1 h, room temp.

3: 91 percent / acetic acid, sodium cyanoborohydride / tetrahydrofuran / 1 h / Ambient temperature

4: 72 percent / pyridine / 24 h / Ambient temperature

5: lithium bis(trimethylsilylamide) / tetrahydrofuran; toluene / 1 h / Ambient temperature

6: CH₂Cl₂ / 0.5 h / Ambient temperature

7: 40 percent / hydrogen, / 10percent palladium on charcoal / tetrahydrofuran; methanol / 15 h / 1520 Torr

8: trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 0.25 h / 0 °C

9: 1.) tosylchloride 2.) triethylamine, KOH / 1.) acetone, 1 h, room temp. 2.) CH₂Cl₂, 2 h, room temp.

With pyridine; potassium hydroxide; dimethylsulfide; trimethylsilyl trifluoromethanesulfonate; hydrogen; sodium cyanoborohydride; ozone; acetic acid; triethylamine; p-toluenesulfonyl chloride; lithium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; toluene;

Reference yield:

: 102192-13-2
<(tert-butoxycarbonyl)amino>-3 (hydroxymethoxymethyl)-4 oxo-2 azetidine-1-acetate de p-nitrobenzyle (3-R,S)(4-R,S)

: 128990-05-6
acide<<(tritylamino-2 thiazolyl-4)(methoxyimino)-acetyl>amino>-7 methoxy-3 oxo-8 thia-4 aza-1 bicyclo<4.2.0> octene-2 carboxylique-2(6-R,S)(7-R,S)(Z)

Guidance literature:: Multi-step reaction with 7 steps

1: 91 percent / acetic acid, sodium cyanoborohydride / tetrahydrofuran / 1 h / Ambient temperature

2: 72 percent / pyridine / 24 h / Ambient temperature

3: lithium bis(trimethylsilylamide) / tetrahydrofuran; toluene / 1 h / Ambient temperature

4: CH₂Cl₂ / 0.5 h / Ambient temperature

5: 40 percent / hydrogen, / 10percent palladium on charcoal / tetrahydrofuran; methanol / 15 h / 1520 Torr

6: trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 0.25 h / 0 °C

7: 1.) tosylchloride 2.) triethylamine, KOH / 1.) acetone, 1 h, room temp. 2.) CH₂Cl₂, 2 h, room temp.

With pyridine; potassium hydroxide; trimethylsilyl trifluoromethanesulfonate; hydrogen; sodium cyanoborohydride; acetic acid; triethylamine; p-toluenesulfonyl chloride; lithium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; toluene;

Reference yield:

: 102192-14-3
<(tert-butoxycarbonyl)amino>-3 hydroxymethyl-4 oxo-2 azetidine-1-acetate de p-nitrobenzyle (3-R,S)(4-R,S)

: 128990-05-6
acide<<(tritylamino-2 thiazolyl-4)(methoxyimino)-acetyl>amino>-7 methoxy-3 oxo-8 thia-4 aza-1 bicyclo<4.2.0> octene-2 carboxylique-2(6-R,S)(7-R,S)(Z)

Guidance literature:: Multi-step reaction with 6 steps

1: 72 percent / pyridine / 24 h / Ambient temperature

2: lithium bis(trimethylsilylamide) / tetrahydrofuran; toluene / 1 h / Ambient temperature

3: CH₂Cl₂ / 0.5 h / Ambient temperature

4: 40 percent / hydrogen, / 10percent palladium on charcoal / tetrahydrofuran; methanol / 15 h / 1520 Torr

5: trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 0.25 h / 0 °C

6: 1.) tosylchloride 2.) triethylamine, KOH / 1.) acetone, 1 h, room temp. 2.) CH₂Cl₂, 2 h, room temp.

With pyridine; potassium hydroxide; trimethylsilyl trifluoromethanesulfonate; hydrogen; triethylamine; p-toluenesulfonyl chloride; lithium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; toluene;