[(3S,4R)-3-Amino-2-oxo-4-((E)-styryl)-azetidin-1-yl]-acetic acid 4-nitro-benzyl ester

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Chemical Name:[(3S,4R)-3-Amino-2-oxo-4-((E)-styryl)-azetidin-1-yl]-acetic acid 4-nitro-benzyl ester
CAS No.:102192-12-1
Molecular Formula:C₂₀H₁₉N₃O₅
Molecular Weight:381.388
Hs Code.:

Synonyms:[(3S,4R)-3-Amino-2-oxo-4-((E)-styryl)-azetidin-1-yl]-acetic acid 4-nitro-benzyl ester

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Chemical Property of [(3S,4R)-3-Amino-2-oxo-4-((E)-styryl)-azetidin-1-yl]-acetic acid 4-nitro-benzyl ester

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Technology Process of [(3S,4R)-3-Amino-2-oxo-4-((E)-styryl)-azetidin-1-yl]-acetic acid 4-nitro-benzyl ester

There total 3 articles about [(3S,4R)-3-Amino-2-oxo-4-((E)-styryl)-azetidin-1-yl]-acetic acid 4-nitro-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 102192-11-0
oxo-2 (phenyl-2 vinyl)-4 phtalimido-3 azetidine-1-acetate de p-nitrobenzyle (3-R,S)(4-S,R)(E)

: 102192-12-1
[(3S,4R)-3-Amino-2-oxo-4-((E)-styryl)-azetidin-1-yl]-acetic acid 4-nitro-benzyl ester

Guidance literature:: With hydrazine hydrate; In 1,4-dioxane; for 1h; Ambient temperature;

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 102192-12-1
[(3S,4R)-3-Amino-2-oxo-4-((E)-styryl)-azetidin-1-yl]-acetic acid 4-nitro-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) magnesium sulfate 2.) triethylamine / 1.) CH₂Cl₂, 30 min, room temp. 2.) CH₂Cl₂, 30 min, reflux

2: 97 percent / hydrazine hydrate / dioxane / 1 h / Ambient temperature

With magnesium sulfate; hydrazine hydrate; triethylamine; In 1,4-dioxane;

Reference yield:

: 7352-64-9
glycine 4-nitrobenzyl ester

: 102192-12-1
[(3S,4R)-3-Amino-2-oxo-4-((E)-styryl)-azetidin-1-yl]-acetic acid 4-nitro-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) magnesium sulfate 2.) triethylamine / 1.) CH₂Cl₂, 30 min, room temp. 2.) CH₂Cl₂, 30 min, reflux

2: 97 percent / hydrazine hydrate / dioxane / 1 h / Ambient temperature

With magnesium sulfate; hydrazine hydrate; triethylamine; In 1,4-dioxane;