2-Propen-1-ol, 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-

Base Information

Chemical Name:2-Propen-1-ol, 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-
CAS No.:608534-39-0
Molecular Formula:C₉H₁₇BO₃
Molecular Weight:184.043
Hs Code.:
DSSTox Substance ID:DTXSID40694700
Mol file:608534-39-0.mol

Synonyms:DTXSID40694700;2-Propen-1-ol, 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-;AB55345

Suppliers and Price of 2-Propen-1-ol, 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(E)-3-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-2-PROPEN-1-OL 95.00%
5MG
$ 500.13

Total 6 raw suppliers

Chemical Property of 2-Propen-1-ol, 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-

Chemical Property:

Vapor Pressure:0.022mmHg at 25°C
Boiling Point:221.436oC at 760 mmHg
PKA:14.85±0.10(Predicted)
Flash Point:87.721°C
PSA：38.69000
Density:0.994g/cm³
LogP:1.16630
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:184.1270746
Heavy Atom Count:13
Complexity:195

Purity/Quality:

98%min ^*data from raw suppliers

(E)-3-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-2-PROPEN-1-OL 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B1(OC(C(O1)(C)C)(C)C)C=CCO

Technology Process of 2-Propen-1-ol, 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-

There total 5 articles about 2-Propen-1-ol, 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: tert-butyldimethyl {[3-(tetramethyl-1,3,2-dioxaborolan-2-yl)prop-2-en-1-yl]oxy}silane

: 608534-39-0
1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-hydroxy-1-propene

Guidance literature:: With activated Dowex-50WX₈; In methanol; for 72h;
DOI:10.1039/c3cc38824g

Reference yield: 85.0%

: 107-19-7
propargyl alcohol

: 73183-34-3
bis(pinacol)diborane

: 608534-39-0
1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-hydroxy-1-propene

Guidance literature:: With C₂₇H₁₉N₂⁽¹⁺⁾*Cl^(1-); 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; at 20 ℃; for 24h; regioselective reaction;
DOI:10.1039/c3ob41499j

Reference yield: 82.0%

: 107-19-7
propargyl alcohol

: 73183-34-3
bis(pinacol)diborane

: 2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)prop-2-en-1-ol

: 608534-39-0
1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-hydroxy-1-propene

Guidance literature:: bis(pinacol)diborane; With (1,3-dimesitylimidazolidin-2-yl)copper(I) chloride; sodium t-butanolate; In tetrahydrofuran; at 22 ℃; for 0.5h; Inert atmosphere;

propargyl alcohol; In tetrahydrofuran; at -50 ℃; for 21h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ja2007643