Technology Process of C19H21NO4
There total 8 articles about C19H21NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine / dichloromethane / 1 h / 0 °C
2: dimethyl sulfoxide / 50 °C
3: palladium 10% on activated carbon; hydrogen / ethyl acetate / 72 h / 760.05 Torr
4: triethylamine; copper diacetate / dichloromethane / 20 °C / Molecular sieve
5: sodium hydroxide / water; ethanol / 3 h / 160 °C
With
palladium 10% on activated carbon; hydrogen; copper diacetate; triethylamine; sodium hydroxide;
In
ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate;
DOI:10.1021/acs.jmedchem.6b01559
- Guidance literature:
-
Multi-step reaction with 6 steps
1: copper(l) iodide; sodium hydroxide / isopropyl alcohol / 90 °C / Inert atmosphere; Sealed tube
2: triethylamine / dichloromethane / 1 h / 0 °C
3: dimethyl sulfoxide / 50 °C
4: palladium 10% on activated carbon; hydrogen / ethyl acetate / 72 h / 760.05 Torr
5: triethylamine; copper diacetate / dichloromethane / 20 °C / Molecular sieve
6: sodium hydroxide / water; ethanol / 3 h / 160 °C
With
copper(l) iodide; palladium 10% on activated carbon; hydrogen; copper diacetate; triethylamine; sodium hydroxide;
In
ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; isopropyl alcohol;
DOI:10.1021/acs.jmedchem.6b01559
