tetrabenzylgermane

Base Information

Chemical Name:tetrabenzylgermane
CAS No.:2816-51-5
Molecular Formula:C₂₈H₂₈Ge
Molecular Weight:437.12
Hs Code.:

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Suppliers and Price of tetrabenzylgermane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetrabenzylgermane

Chemical Property:

Vapor Pressure:2.11E-11mmHg at 25°C

Purity/Quality:

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Technology Process of tetrabenzylgermane

There total 5 articles about tetrabenzylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 112712-64-8
tris(1,2-benzenediolato-O,O′)germanate

: 1589-82-8
phenylmagnesium bromide

: 2816-51-5
tetrabenzylgermanium

Guidance literature:: In diethyl ether; (N2); added dropwise a soln. of C6H5CH2MgBr to a suspn. of Ge-compound; stirred for 1 h at room temp.; hydrolyzed; extracted with ether; washed with water; dried over MgSO4; evapd.; recrystd. from ethanol;
DOI:10.1021/om00051a049

Reference yield: 50.0%

: 112712-64-8
tris(1,2-benzenediolato-O,O′)germanate

: 100-39-0
benzyl bromide

: 2816-51-5
tetrabenzylgermanium

Guidance literature:: With magnesium; In tetrahydrofuran; byproducts: dibenzyl; (N2); heated a suspn. of Mg and Ge-compound under stirring to 50-55°C; added dropwise a soln. of benzyl bromide; refluxed under stirring for 2 h; cooled; added ether; evapd.; washed with pentane; recrystd. from ethanol;
DOI:10.1021/om00051a049