Technology Process of C28H30N4O7S2
There total 5 articles about C28H30N4O7S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: caesium carbonate; tris-(dibenzylideneacetone)dipalladium(0); 1,1'-bi-2-naphthol / toluene / 100 °C
2: water; lithium hydroxide / tetrahydrofuran / 20 °C
3: triethylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / N,N-dimethyl-formamide; dichloromethane
With
tris-(dibenzylideneacetone)dipalladium(0); water; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; triethylamine; lithium hydroxide; 1,1'-bi-2-naphthol;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2013.06.027
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogenchloride; water
2: caesium carbonate; tris-(dibenzylideneacetone)dipalladium(0); 1,1'-bi-2-naphthol / toluene / 100 °C
3: water; lithium hydroxide / tetrahydrofuran / 20 °C
4: triethylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / N,N-dimethyl-formamide; dichloromethane
With
hydrogenchloride; tris-(dibenzylideneacetone)dipalladium(0); water; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; triethylamine; lithium hydroxide; 1,1'-bi-2-naphthol;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2013.06.027
- Guidance literature:
-
Multi-step reaction with 5 steps
1: ammonia / methanol; water-d2 / 0 - 20 °C
2: hydrogenchloride; water
3: caesium carbonate; tris-(dibenzylideneacetone)dipalladium(0); 1,1'-bi-2-naphthol / toluene / 100 °C
4: water; lithium hydroxide / tetrahydrofuran / 20 °C
5: triethylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / N,N-dimethyl-formamide; dichloromethane
With
hydrogenchloride; tris-(dibenzylideneacetone)dipalladium(0); ammonia; water; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; triethylamine; lithium hydroxide; 1,1'-bi-2-naphthol;
In
tetrahydrofuran; methanol; dichloromethane; water-d2; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2013.06.027