threo-3-(p-carboxyphenyl)-4-(p-hydroxyphenyl)hexane

Base Information

Chemical Name:threo-3-(p-carboxyphenyl)-4-(p-hydroxyphenyl)hexane
CAS No.:39952-75-5
Molecular Formula:C₁₉H₂₂O₃
Molecular Weight:298.382
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of threo-3-(p-carboxyphenyl)-4-(p-hydroxyphenyl)hexane

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Technology Process of threo-3-(p-carboxyphenyl)-4-(p-hydroxyphenyl)hexane

There total 20 articles about threo-3-(p-carboxyphenyl)-4-(p-hydroxyphenyl)hexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 76412-22-1
erythro-3--4-(p-carboxyphenyl)hexane

: 39952-75-5,76412-37-8
erythro-3-(p-carboxyphenyl)-4-(p-hydroxyphenyl)hexane

Guidance literature:: With potassium carbonate; In methanol; at 25 ℃; for 18h;
DOI:10.1021/jm00136a013

Reference yield:

: 84-16-2,26614-21-1
hexestrol

: 39952-75-5,76412-37-8
erythro-3-(p-carboxyphenyl)-4-(p-hydroxyphenyl)hexane

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) K₂CO₃, 2.) H₂ / 2.) 5percent Pd/C / 1.) acetone, reflux, 17 h, 2.) ethanol, 37 psi, 35 deg C

2: 90 percent / pyridine / Ambient temperature

3: 66 percent / AlCl₃ / CS₂ / 6 h / Heating

4: 94 percent / 1.4 M aq. KOCl / dioxane / 0.5 h / 60 °C

5: 96 percent / K₂CO₃ / methanol / 18 h / 25 °C

With pyridine; aluminium trichloride; potassium hypochlorite; hydrogen; potassium carbonate; palladium on activated charcoal; In 1,4-dioxane; methanol; carbon disulfide;
DOI:10.1021/jm00136a013