O-ethyl N,N-diethyl-P-benzylphosphonamidate

Base Information

Chemical Name:O-ethyl N,N-diethyl-P-benzylphosphonamidate
CAS No.:27272-09-9
Molecular Formula:C₁₃H₂₂NO₂P
Molecular Weight:255.297
Hs Code.:

Synonyms:

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Chemical Property of O-ethyl N,N-diethyl-P-benzylphosphonamidate

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Technology Process of O-ethyl N,N-diethyl-P-benzylphosphonamidate

There total 7 articles about O-ethyl N,N-diethyl-P-benzylphosphonamidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 27272-09-9
O-ethyl N,N-diethyl-P-benzylphosphonamidate

Guidance literature:: Multi-step reaction with 4 steps

1: 0.33 h / 140 °C / Inert atmosphere; Microwave irradiation

2: sodium hydroxide / water / 0.33 h / Reflux; Microwave irradiation

3: triethylamine; 1-[(1-(cyano-?2-?ethoxy-?2-?oxoethylidenaminooxy)?dimethylamino-?morpholino)]-uronium hexafluorophosphate / dichloromethane / 2 h / 20 - 22 °C

4: dichloromethane / 4 h

With 1-[(1-(cyano-?2-?ethoxy-?2-?oxoethylidenaminooxy)?dimethylamino-?morpholino)]-uronium hexafluorophosphate; triethylamine; sodium hydroxide; In dichloromethane; water;
DOI:10.1002/ejoc.201501244

Reference yield:

: 18933-98-7
benzylphosphonic acid monoethyl ester

: 27272-09-9
O-ethyl N,N-diethyl-P-benzylphosphonamidate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; 1-[(1-(cyano-?2-?ethoxy-?2-?oxoethylidenaminooxy)?dimethylamino-?morpholino)]-uronium hexafluorophosphate / dichloromethane / 2 h / 20 - 22 °C

2: dichloromethane / 4 h

With 1-[(1-(cyano-?2-?ethoxy-?2-?oxoethylidenaminooxy)?dimethylamino-?morpholino)]-uronium hexafluorophosphate; triethylamine; In dichloromethane;
DOI:10.1002/ejoc.201501244

Reference yield:

: 1080-32-6
O,O-diethyl benzylphosphonate

: 27272-09-9
O-ethyl N,N-diethyl-P-benzylphosphonamidate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / water / 0.33 h / Reflux; Microwave irradiation

2: triethylamine; 1-[(1-(cyano-?2-?ethoxy-?2-?oxoethylidenaminooxy)?dimethylamino-?morpholino)]-uronium hexafluorophosphate / dichloromethane / 2 h / 20 - 22 °C

3: dichloromethane / 4 h

With 1-[(1-(cyano-?2-?ethoxy-?2-?oxoethylidenaminooxy)?dimethylamino-?morpholino)]-uronium hexafluorophosphate; triethylamine; sodium hydroxide; In dichloromethane; water;
DOI:10.1002/ejoc.201501244