(+)-(9S,10S)-trans-10-Bromo-9-(p-methoxybenzoyloxy)-9,10,11,12-tetrahydrobenzopyrene

Base Information

Chemical Name:(+)-(9S,10S)-trans-10-Bromo-9-(p-methoxybenzoyloxy)-9,10,11,12-tetrahydrobenzopyrene
CAS No.:88780-81-8
Molecular Formula:C₂₈H₂₁BrO₃
Molecular Weight:485.377
Hs Code.:

(+)-(9S,10S)-trans-10-Bromo-9-(p-methoxybenzoyloxy)-9,10,11,12-tetrahydrobenzo<e>pyrene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-(9S,10S)-trans-10-Bromo-9-(p-methoxybenzoyloxy)-9,10,11,12-tetrahydrobenzopyrene

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Technology Process of (+)-(9S,10S)-trans-10-Bromo-9-(p-methoxybenzoyloxy)-9,10,11,12-tetrahydrobenzopyrene

There total 3 articles about (+)-(9S,10S)-trans-10-Bromo-9-(p-methoxybenzoyloxy)-9,10,11,12-tetrahydrobenzopyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 88824-51-5
(+)-(9S,10S)-trans-10-Bromo-9-hydroxy-9,10,11,12-tetrahydrobenzopyrene

: 100-07-2
4-methoxy-benzoyl chloride

: 88780-81-8
(+)-(9S,10S)-trans-10-Bromo-9-(p-methoxybenzoyloxy)-9,10,11,12-tetrahydrobenzopyrene

Guidance literature:: With pyridine; Ambient temperature;
DOI:10.1021/jo00180a030

Reference yield:

: 66788-01-0
9,10-Dihydrobenzopyrene

: 88780-81-8
(+)-(9S,10S)-trans-10-Bromo-9-(p-methoxybenzoyloxy)-9,10,11,12-tetrahydrobenzopyrene

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / NBS / dimethylsulfoxide / 1 h / Ambient temperature

2: pyridine / Ambient temperature

3: 99 percent / LiAlH₄ / diethyl ether / 0.5 h / Ambient temperature

4: 99 percent / pyridine / Ambient temperature

With pyridine; N-Bromosuccinimide; lithium aluminium tetrahydride; In diethyl ether; dimethyl sulfoxide;
DOI:10.1021/jo00180a030

Reference yield:

: 88767-14-0
(+/-)-trans-10-Bromo-9-hydroxy-9,10,11,12-tetrahydrobenzopyrene

: 88780-81-8
(+)-(9S,10S)-trans-10-Bromo-9-(p-methoxybenzoyloxy)-9,10,11,12-tetrahydrobenzopyrene

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / Ambient temperature

2: 99 percent / LiAlH₄ / diethyl ether / 0.5 h / Ambient temperature

3: 99 percent / pyridine / Ambient temperature

With pyridine; lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1021/jo00180a030