S,S-dimethyl-N-(3-pyridyl)sulfinimine

Base Information

Chemical Name:S,S-dimethyl-N-(3-pyridyl)sulfinimine
CAS No.:156544-61-5
Molecular Formula:C₇H₉ClN₂S
Molecular Weight:188.681
Hs Code.:
Mol file:156544-61-5.mol

Synonyms:

Suppliers and Price of S,S-dimethyl-N-(3-pyridyl)sulfinimine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of S,S-dimethyl-N-(3-pyridyl)sulfinimine

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of S,S-dimethyl-N-(3-pyridyl)sulfinimine

There total 1 articles about S,S-dimethyl-N-(3-pyridyl)sulfinimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 6298-19-7
2-chloro-3-aminopyridine

: 75-18-3
dimethylsulfide

: 156544-61-5
S,S-dimethyl-N-(3-pyridyl)sulfinimine

Guidance literature:: With N-chloro-succinimide; In dichloromethane; at 0 - 5 ℃; for 1h;
DOI:10.1002/jhet.5570370203

Reference yield:

: 156544-61-5
S,S-dimethyl-N-(3-pyridyl)sulfinimine

: 133627-24-4
11-cyclopropyl-5,11-dihydro-4-(hydroxymethyl)-6H-dipyrido<3,2-b:2',3'-e><1,4>diazepine-6-one

Guidance literature:: Multi-step reaction with 8 steps

1.1: 56 percent / 2-t-butyl-4-methylphenol / toluene / 2 h / 90 - 95 °C

2.1: 49 percent / sodium carbonate / toluene / 2 h / 90 - 100 °C

3.1: 83.6 percent / xylene / 72 h / 105 °C

4.1: 54 percent / sodium hydride; pyridine / 1 h / 75 - 85 °C

5.1: trifluoroacetic acid / 168 h

6.1: sodium hydride / tetrahydrofuran / 0.25 h / -78 °C

6.2: tetrahydrofuran / 1 h / 20 °C

7.1: 28 percent / sodium iodide; trifluoroacetic acid / acetonitrile / 0 °C

8.1: ozone / methanol / 0.17 h / -40 °C

8.2: methyl sulfide / methanol

8.3: 45 percent / sodium borohydride / methanol / 2 h / 0 °C

With pyridine; 2-tert-Butyl-4-methylphenol; sodium hydride; sodium carbonate; ozone; trifluoroacetic acid; sodium iodide; In tetrahydrofuran; methanol; toluene; acetonitrile; xylene; 1.1: Rearrangement / 2.1: Condensation / 3.1: Substitution / 4.1: Cyclization / 5.1: Alkylation / 6.1: Reduction / 6.2: Epoxidation / 7.1: Elimination / 8.1: Oxidation / 8.2: Reduction / 8.3: Reduction;
DOI:10.1002/jhet.5570370203