anti 7-benzhydrylbicyclo<2.2.1>hepta-2-one

Base Information

Chemical Name:anti 7-benzhydrylbicyclo<2.2.1>hepta-2-one
CAS No.:92973-94-9
Molecular Formula:C₂₀H₂₀O
Molecular Weight:276.378
Hs Code.:

Synonyms:

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Chemical Property of anti 7-benzhydrylbicyclo<2.2.1>hepta-2-one

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Technology Process of anti 7-benzhydrylbicyclo<2.2.1>hepta-2-one

There total 6 articles about anti 7-benzhydrylbicyclo<2.2.1>hepta-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 92973-92-7
7-benzhydrylidenebicyclo<2.2.1>heptan-2-one

: 92973-94-9,92973-95-0
anti 7-benzhydrylbicyclo<2.2.1>hepta-2-one

Guidance literature:: With palladium on activated charcoal; hydrogen; In ethanol; for 48h; under 760 Torr; Yields of byproduct given;

Reference yield:

: 119-61-9
benzophenone

: 92973-94-9,92973-95-0
anti 7-benzhydrylbicyclo<2.2.1>hepta-2-one

Guidance literature:: Multi-step reaction with 5 steps

1: 82 percent / sodium ethoxide / ethanol / 3.5 h

2: benzene / 1848 h / 40 °C

3: 5percent Pd/C, H₂ / ethyl acetate / 760 Torr

4: 86 percent / aq. potassium hydroxide / dimethylsulfoxide / 13 h

5: 10percent Pd/C, H₂ / ethanol / 48 h / 760 Torr

With potassium hydroxide; palladium on activated charcoal; hydrogen; sodium ethanolate; In ethanol; dimethyl sulfoxide; ethyl acetate; benzene;

Reference yield:

: 7714-72-9
6,6-diphenylfulvene

: 92973-94-9,92973-95-0
anti 7-benzhydrylbicyclo<2.2.1>hepta-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: benzene / 1848 h / 40 °C

2: 5percent Pd/C, H₂ / ethyl acetate / 760 Torr

3: 86 percent / aq. potassium hydroxide / dimethylsulfoxide / 13 h

4: 10percent Pd/C, H₂ / ethanol / 48 h / 760 Torr

With potassium hydroxide; palladium on activated charcoal; hydrogen; In ethanol; dimethyl sulfoxide; ethyl acetate; benzene;