Benzoic acid (S)-1-[(2S,5R)-5-((3aS,5S,6R,6aS)-6-benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-tetrahydro-furan-2-yl]-undecyl ester

Base Information

Chemical Name:Benzoic acid (S)-1-[(2S,5R)-5-((3aS,5S,6R,6aS)-6-benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-tetrahydro-furan-2-yl]-undecyl ester
CAS No.:144368-11-6
Molecular Formula:C₃₆H₅₀O₇
Molecular Weight:594.789
Hs Code.:

Benzoic acid (S)-1-[(2S,5R)-5-((3aS,5S,6R,6aS)-6-benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-tetrahydro-furan-2-yl]-undecyl ester

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Chemical Property of Benzoic acid (S)-1-[(2S,5R)-5-((3aS,5S,6R,6aS)-6-benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-tetrahydro-furan-2-yl]-undecyl ester

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Technology Process of Benzoic acid (S)-1-[(2S,5R)-5-((3aS,5S,6R,6aS)-6-benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-tetrahydro-furan-2-yl]-undecyl ester

There total 8 articles about Benzoic acid (S)-1-[(2S,5R)-5-((3aS,5S,6R,6aS)-6-benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-tetrahydro-furan-2-yl]-undecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 765-03-7
1-dodecyne

: 144368-11-6,144489-83-8
Benzoic acid (S)-1-[(2S,5R)-5-((3aS,5S,6R,6aS)-6-benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-tetrahydro-furan-2-yl]-undecyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) BuLi

2: pyridine

3: MgBr / diethyl ether

4: 1.) MgBr / 1.) ether

5: Lindlar reduction

6: metachloroperbenzoic acid / CH₂Cl₂

7: AcOH / CH₂Cl₂ / 12 h / 20 °C

8: benzoylation

With pyridine; n-butyllithium; acetic acid; 3-chloro-benzenecarboperoxoic acid; magnesium bromide; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4039(00)79126-X

Reference yield:

: 55182-74-6
1-hydroxy-tetradec-3-yne

: 144368-11-6,144489-83-8
Benzoic acid (S)-1-[(2S,5R)-5-((3aS,5S,6R,6aS)-6-benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-tetrahydro-furan-2-yl]-undecyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine

2: MgBr / diethyl ether

3: 1.) MgBr / 1.) ether

4: Lindlar reduction

5: metachloroperbenzoic acid / CH₂Cl₂

6: AcOH / CH₂Cl₂ / 12 h / 20 °C

7: benzoylation

With pyridine; acetic acid; 3-chloro-benzenecarboperoxoic acid; magnesium bromide; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4039(00)79126-X

Reference yield:

: 144368-18-3
1-bromo-tetradec-3-yne

: 144368-11-6,144489-83-8
Benzoic acid (S)-1-[(2S,5R)-5-((3aS,5S,6R,6aS)-6-benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-tetrahydro-furan-2-yl]-undecyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) MgBr / 1.) ether

2: Lindlar reduction

3: metachloroperbenzoic acid / CH₂Cl₂

4: AcOH / CH₂Cl₂ / 12 h / 20 °C

5: benzoylation

With acetic acid; 3-chloro-benzenecarboperoxoic acid; magnesium bromide; In dichloromethane;
DOI:10.1016/S0040-4039(00)79126-X