C₂₉H₄₆O₆S₃

Base Information

Chemical Name:C₂₉H₄₆O₆S₃
CAS No.:943322-84-7
Molecular Formula:C₂₉H₄₆O₆S₃
Molecular Weight:586.879
Hs Code.:

C<sub>29</sub>H<sub>46</sub>O<sub>6</sub>S<sub>3</sub>

Synonyms:

Suppliers and Price of C₂₉H₄₆O₆S₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₉H₄₆O₆S₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₉H₄₆O₆S₃

There total 12 articles about C₂₉H₄₆O₆S₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 943322-54-1
C₁₄H₂₄O₄S₂

: 6553-96-4
2,4,6-triisopropylphenylsulfonyl chloride

: 943322-84-7
C₂₉H₄₆O₆S₃

Guidance literature:: With dmap; In dichloromethane; at 50 ℃; for 2.5h;
DOI:10.1016/j.tet.2007.03.144

Reference yield:

: 1941-50-0
D-arabinose diethyl dithioacetal

: 943322-84-7
C₂₉H₄₆O₆S₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: 92 percent / concd. H₂SO₄

2.1: 82 percent / CeCl₃*7H₂O; oxalic acid / acetonitrile / 20 °C

3.1: 77 percent / Et₃N / CH₂Cl₂ / 20 °C

4.1: 95 percent / imidazole / dimethylformamide / 20 °C

5.1: 91 percent / DIBAL-H / cyclohexane; CH₂Cl₂ / 0.5 h / -78 °C

6.1: 82 percent / SO₃*Py; i-Pr₂NEt / dimethylsulfoxide; CH₂Cl₂ / 0 - 20 °C

7.1: n-BuLi / hexane; tetrahydrofuran / 0.25 h / -78 °C

7.2: 547 mg / hexane; tetrahydrofuran / 3 h / -78 °C

8.1: 95 percent / K₂CO₃ / methanol; tetrahydrofuran / 0.5 h / cooling

9.1: DMAP / CH₂Cl₂ / 2.5 h / 50 °C

With 1H-imidazole; dmap; n-butyllithium; cerium(III) chloride; pyridine-SO₃ complex; sulfuric acid; oxalic acid; diisobutylaluminium hydride; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; hexane; dichloromethane; cyclohexane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2007.03.144

Reference yield:

: 28697-53-2
D-arabinopyranose

: 943322-84-7
C₂₉H₄₆O₆S₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: 78 percent / aq. HCl

2.1: 92 percent / concd. H₂SO₄

3.1: 82 percent / CeCl₃*7H₂O; oxalic acid / acetonitrile / 20 °C

4.1: 77 percent / Et₃N / CH₂Cl₂ / 20 °C

5.1: 95 percent / imidazole / dimethylformamide / 20 °C

6.1: 91 percent / DIBAL-H / cyclohexane; CH₂Cl₂ / 0.5 h / -78 °C

7.1: 82 percent / SO₃*Py; i-Pr₂NEt / dimethylsulfoxide; CH₂Cl₂ / 0 - 20 °C

8.1: n-BuLi / hexane; tetrahydrofuran / 0.25 h / -78 °C

8.2: 547 mg / hexane; tetrahydrofuran / 3 h / -78 °C

9.1: 95 percent / K₂CO₃ / methanol; tetrahydrofuran / 0.5 h / cooling

10.1: DMAP / CH₂Cl₂ / 2.5 h / 50 °C

With 1H-imidazole; hydrogenchloride; dmap; n-butyllithium; cerium(III) chloride; pyridine-SO₃ complex; sulfuric acid; oxalic acid; diisobutylaluminium hydride; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; hexane; dichloromethane; cyclohexane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2007.03.144