trans-1,2-epoxy-1,3-diphenylpropane

Base Information

• Chemical Name: trans-1,2-epoxy-1,3-diphenylpropane
• CAS No.: 65095-04-7
• Molecular Formula: C₁₅H₁₄O
• Molecular Weight: 210.276
• Mol file: 65095-04-7.mol

Synonyms:

Chemical Property of trans-1,2-epoxy-1,3-diphenylpropane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of trans-1,2-epoxy-1,3-diphenylpropane

There total 12 articles about trans-1,2-epoxy-1,3-diphenylpropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

(1E)-1,3-diphenylpropene (3412-44-0) → trans-1,2-epoxy-1,3-diphenylpropane (65095-03-6,65095-04-7)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; 1.) 0 deg C, 30 min; 2.) room temperature, 12 h;

DOI:10.1039/P29860000923

Reference yield: 80.0%

phenyldiazomethane (908094-04-2) + phenylacetaldehyde (122-78-1) → trans-1,2-epoxy-1,3-diphenylpropane (65095-03-6,65095-04-7)

Guidance literature:

With dirhodium tetraacetate; dimethylsulfide; In dichloromethane; for 24h;

Reference yield: 60.0%

phenylacetaldehyde (122-78-1) + sodium (E)-2-benzylidene-1-tosylhydrazin-1-ide → trans-1,2-epoxy-1,3-diphenylpropane (65095-03-6,65095-04-7)

Guidance literature:

With thiophene; dirhodium tetraacetate; N-benzyl-N,N,N-triethylammonium chloride; In acetonitrile; at 40 ℃; for 24h;

DOI:10.1021/ja034606+

upstream raw materials:

(1E)-1,3-diphenylpropene

phenyldiazomethane

phenylacetaldehyde

1,1-diiodo-2-phenylethane

Downstream raw materials:

(E)-1,3-diphenyl-2-propen-1-ol

1,3-diphenylpropane-1,2-diol