{(Mo(CO)3(PPh2Me)(η4-C4Ph4CO))}

Base Information

Chemical Name:{(Mo(CO)3(PPh2Me)(η4-C4Ph4CO))}
CAS No.:147281-44-5
Molecular Formula:C₄₅H₃₃MoO₄P
Molecular Weight:764.668
Hs Code.:

Synonyms:

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Chemical Property of {(Mo(CO)3(PPh2Me)(η4-C4Ph4CO))}

Chemical Property:

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Technology Process of {(Mo(CO)3(PPh2Me)(η4-C4Ph4CO))}

There total 3 articles about {(Mo(CO)3(PPh2Me)(η4-C4Ph4CO))} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 147281-42-3
{(Mo(CO)3(NCMe)(η4-C4Ph4CO))}

: 1486-28-8
diphenyl(methyl)phosphine

: 147281-44-5
{(Mo(CO)3(PPh2Me)(η4-C4Ph4CO))}

Guidance literature:: In dichloromethane; stirring of (Mo(CO)3(NCMe)(C4Ph4CO)) and PPh2Me in CH2Cl2 for 18 h;; chromy. (CH2Cl2 and CH2Cl2/acetone (19:1)); elem. anal.;;
DOI:10.1039/DT9930000091

Reference yield: 79.0%

: 108241-82-3
{Mo(CO)2(η4-C4Ph4CO)2}

: 1486-28-8
diphenyl(methyl)phosphine

: 147281-44-5
{(Mo(CO)3(PPh2Me)(η4-C4Ph4CO))}

Guidance literature:: In toluene; byproducts: tetracyclone; refluxing of (Mo(CO)2(C4Ph4CO)2) with 2 equivalents of PPh2Me in toluene for 18 h;; column chromy. (CH2Cl2/acetone (19:1));;
DOI:10.1039/DT9930000091

Reference yield:

: 479-33-4
2,3,4,5-tetraphenylcyclopenta-2,4-dienone

: 1486-28-8
diphenyl(methyl)phosphine

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 147281-44-5
{(Mo(CO)3(PPh2Me)(η4-C4Ph4CO))}

Guidance literature:: In tetrahydrofuran; byproducts: tetracyclone; refluxing of Mo(CO)6 in CH3CN for 5 h; the solvent was removed and the residue was suspended in THF; treatment with tetracyclone; addn. of PPh2Me;; chromy.;;
DOI:10.1039/DT9930000091