{(Mo(CO)3(NCMe)(η4-C4Ph4CO))}

Base Information

Chemical Name:{(Mo(CO)3(NCMe)(η4-C4Ph4CO))}
CAS No.:147281-42-3
Molecular Formula:C₃₄H₂₃MoNO₄
Molecular Weight:605.501
Hs Code.:

Synonyms:{(Mo(CO)3(NCMe)(η4-C4Ph4CO))}

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Chemical Property of {(Mo(CO)3(NCMe)(η4-C4Ph4CO))}

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Technology Process of {(Mo(CO)3(NCMe)(η4-C4Ph4CO))}

There total 1 articles about {(Mo(CO)3(NCMe)(η4-C4Ph4CO))} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 479-33-4
2,3,4,5-tetraphenylcyclopenta-2,4-dienone

: 75-05-8,26809-02-9
acetonitrile

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 147281-42-3
{(Mo(CO)3(NCMe)(η4-C4Ph4CO))}

Guidance literature:: In tetrahydrofuran; refluxing of Mo(CO)6 in CH3CN for 5 h; removal of solvent; the residue was dissolved in THF and solid tetracyclone was added; stirring for 18 h;; the soln. was concd. and overlayered with hexane; crystn. at -20°C over a period of 3 d; elem. anal.;;
DOI:10.1039/DT9930000091

Reference yield: 96.0%

: 147281-42-3
{(Mo(CO)3(NCMe)(η4-C4Ph4CO))}

: 147281-43-4
{(Mo(CO)3(PPh3)(η4-C4Ph4CO))}

Guidance literature:: With triphenyl phosphine; In dichloromethane; byproducts: tetracyclone; stirring of (Mo(CO)3(NCMe)(C4Ph4CO)) and PPh3 in CH2Cl2 for 18 h;; removal of solvent; the residue was washed with hexane; elem. anal. for (Mo(CO)3(PPh3)(C4Ph4CO))*0.5CH3COOC2H5;;
DOI:10.1039/DT9930000091

Reference yield: 96.0%

: 147281-42-3
{(Mo(CO)3(NCMe)(η4-C4Ph4CO))}

: 829-85-6
diphenylphosphane

: 147281-45-6
{(Mo(CO)3(PPh2H)(η4-C4Ph4CO))}

Guidance literature:: In dichloromethane; byproducts: tetracyclone; stirring of (Mo(CO)3(NCMe)(C4Ph4CO)) and PPh2H in CH2Cl2 for 18 h;; chromy. (CH2Cl2 and CH2Cl2/acetone (19:1)); elem. anal.;;
DOI:10.1039/DT9930000091