SbF₃(OAs(C₆H₅)3)2

Base Information

• Chemical Name: SbF₃(OAs(C₆H₅)3)2
• CAS No.: 1310057-16-9
• Molecular Formula: C₃₆H₃₀As₂F₃O₂Sb
• Molecular Weight: 823.221
• Mol file: 1310057-16-9.mol

Synonyms:

Chemical Property of SbF₃(OAs(C₆H₅)3)2

Chemical Property:

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Technology Process of SbF₃(OAs(C₆H₅)3)2

There total 1 articles about SbF₃(OAs(C₆H₅)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

triphenylarsineoxide (1153-05-5,856568-31-5) + antimony(III) fluoride (7783-56-4) → SbF3(OAs(C6H5)3)2 (59232-16-5,1310057-16-9)

Guidance literature:

In methanol; byproducts: (C6H5)3AsF2; (N2); dropwise addn. of a soln. of arsine oxide in methanol to a soln. of SbF3 in methanol, stirring overnight; concn. in vac., filtration, washing ppt. with n-hexane, drying in vac., freezing the filtrate; elem. anal.;

DOI:10.1039/c1dt10113g

upstream raw materials:

triphenylarsineoxide

antimony(III) fluoride