2,3,6,2',3',4',6'-hepta-O-benzyl-α-lactosyl bromide

Base Information

Chemical Name:2,3,6,2',3',4',6'-hepta-O-benzyl-α-lactosyl bromide
CAS No.:126777-86-4
Molecular Formula:C₆₁H₆₃BrO₁₀
Molecular Weight:1036.07
Hs Code.:

Synonyms:

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Chemical Property of 2,3,6,2',3',4',6'-hepta-O-benzyl-α-lactosyl bromide

Chemical Property:

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Technology Process of 2,3,6,2',3',4',6'-hepta-O-benzyl-α-lactosyl bromide

There total 4 articles about 2,3,6,2',3',4',6'-hepta-O-benzyl-α-lactosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126777-85-3
2-methoxyethyl O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1<*>4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 126777-86-4
2,3,6,2',3',4',6'-hepta-O-benzyl-α-lactosyl bromide

Guidance literature:: With titanium(IV) bromide; In dichloromethane; for 0.0833333h; Ambient temperature;
DOI:10.1016/0008-6215(89)85109-2

Reference yield:

: 100-44-7
benzyl chloride

: 126777-86-4
2,3,6,2',3',4',6'-hepta-O-benzyl-α-lactosyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / KOH / toluene / 0.5 h / Heating

2: TiBr₄ / CH₂Cl₂ / 0.08 h / Ambient temperature

With potassium hydroxide; titanium(IV) bromide; In dichloromethane; toluene;
DOI:10.1016/0008-6215(89)85109-2

Reference yield:

: 126777-84-2
2-methoxyethyl O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1<*>4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

: 126777-86-4
2,3,6,2',3',4',6'-hepta-O-benzyl-α-lactosyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / KOH / toluene / 0.5 h / Heating

2: TiBr₄ / CH₂Cl₂ / 0.08 h / Ambient temperature

With potassium hydroxide; titanium(IV) bromide; In dichloromethane; toluene;
DOI:10.1016/0008-6215(89)85109-2