1,5-anhydro-2,3,6-tri-O-benzyl-4-O-(2′,3′,4′,6′-tetra-O-benzyl-β-D-galactopyranosyl)-D-arabino-hex-1-enitol

Base Information

Chemical Name:1,5-anhydro-2,3,6-tri-O-benzyl-4-O-(2′,3′,4′,6′-tetra-O-benzyl-β-D-galactopyranosyl)-D-arabino-hex-1-enitol
CAS No.:126777-88-6
Molecular Formula:C₆₁H₆₂O₁₀
Molecular Weight:955.157
Hs Code.:

Synonyms:1,5-anhydro-2,3,6-tri-O-benzyl-4-O-(2′,3′,4′,6′-tetra-O-benzyl-β-D-galactopyranosyl)-D-arabino-hex-1-enitol

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Chemical Property of 1,5-anhydro-2,3,6-tri-O-benzyl-4-O-(2′,3′,4′,6′-tetra-O-benzyl-β-D-galactopyranosyl)-D-arabino-hex-1-enitol

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Technology Process of 1,5-anhydro-2,3,6-tri-O-benzyl-4-O-(2′,3′,4′,6′-tetra-O-benzyl-β-D-galactopyranosyl)-D-arabino-hex-1-enitol

There total 11 articles about 1,5-anhydro-2,3,6-tri-O-benzyl-4-O-(2′,3′,4′,6′-tetra-O-benzyl-β-D-galactopyranosyl)-D-arabino-hex-1-enitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1202532-50-0
C₆₁H₆₃ClO₁₀

: 126777-88-6
1,5-anhydro-2,3,6-tri-O-benzyl-4-O-(2′,3′,4′,6′-tetra-O-benzyl-β-D-galactopyranosyl)-D-arabino-hex-1-enitol

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In acetonitrile; at 85 ℃; for 2h; Molecular sieve;
DOI:10.1021/jo901945e

Reference yield: 25.3%

: 62067-18-9
1-O-acetyl-2-O-benzyl-(R,S)-glycerol

: 126777-86-4
2,3,6,2',3',4',6'-hepta-O-benzyl-α-lactosyl bromide

: 126777-88-6
1,5-anhydro-2,3,6-tri-O-benzyl-4-O-(2′,3′,4′,6′-tetra-O-benzyl-β-D-galactopyranosyl)-D-arabino-hex-1-enitol

: 126777-87-5,126873-13-0
3-O-acetyl-2-O-benzyl-1-O-(2,3,6,2',3',4',6'-hepta-O-benzyl-α-lactosyl)-(R,S)-glycerol

Guidance literature:: With 4 A molecular sieve; tetraethylammonium bromide; In 1,2-dichloro-ethane; RT, 3 h, 75/80 deg C, 41 h, RT, 48 h;
DOI:10.1016/0008-6215(89)85109-2

Reference yield: 20.4%

: 126777-86-4
2,3,6,2',3',4',6'-hepta-O-benzyl-α-lactosyl bromide

: 126777-88-6
1,5-anhydro-2,3,6-tri-O-benzyl-4-O-(2′,3′,4′,6′-tetra-O-benzyl-β-D-galactopyranosyl)-D-arabino-hex-1-enitol

: 126777-87-5,126873-13-0
3-O-acetyl-2-O-benzyl-1-O-(2,3,6,2',3',4',6'-hepta-O-benzyl-α-lactosyl)-(R,S)-glycerol

Guidance literature:: With 4 A molecular sieve; 1-O-acetyl-2-O-benzyl-(R,S)-glycerol; tetraethylammonium bromide; In 1,2-dichloro-ethane; RT, 3 h, 75/80 deg C, 41 h, RT, 48 h;
DOI:10.1016/0008-6215(89)85109-2