1,4-Dimethyl-2-((R)-3-methyl-pent-4-enyl)-benzene

Base Information

Chemical Name:1,4-Dimethyl-2-((R)-3-methyl-pent-4-enyl)-benzene
CAS No.:130323-74-9
Molecular Formula:C₁₄H₂₀
Molecular Weight:188.313
Hs Code.:

Synonyms:

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Chemical Property of 1,4-Dimethyl-2-((R)-3-methyl-pent-4-enyl)-benzene

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Technology Process of 1,4-Dimethyl-2-((R)-3-methyl-pent-4-enyl)-benzene

There total 6 articles about 1,4-Dimethyl-2-((R)-3-methyl-pent-4-enyl)-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63473-60-9
(R)-3-methylpentanedioic acid monomethyl ester

: 130323-74-9
1,4-Dimethyl-2-((R)-3-methyl-pent-4-enyl)-benzene

Guidance literature:: Multi-step reaction with 5 steps

1: Ph₃P / CH₂Cl₂ / 36 h

2: 1.) Li, CuI / 1.) Et₂O, -78 to 0 deg C; 2.) -78 deg C, 30 min

3: LiAlH₄ / diethyl ether

4: H₂, HClO₄ / 10percent Pd/C / ethanol / 15 h / 760 Torr

5: 1.) n-Bu₃P, o-NO₂-C₆H₄-SeCN; 2.) 30 percent H₂O₂

With copper(l) iodide; lithium aluminium tetrahydride; perchloric acid; ortho-nitrophenyl selenocyanate; tributylphosphine; hydrogen; dihydrogen peroxide; lithium; triphenylphosphine; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane;
DOI:10.1016/0040-4039(90)80114-2

Reference yield:

: 19013-37-7
dimethyl 3-methylglutarate

: 130323-74-9
1,4-Dimethyl-2-((R)-3-methyl-pent-4-enyl)-benzene

Guidance literature:: Multi-step reaction with 6 steps

1: pig liver esterase

2: Ph₃P / CH₂Cl₂ / 36 h

3: 1.) Li, CuI / 1.) Et₂O, -78 to 0 deg C; 2.) -78 deg C, 30 min

4: LiAlH₄ / diethyl ether

5: H₂, HClO₄ / 10percent Pd/C / ethanol / 15 h / 760 Torr

6: 1.) n-Bu₃P, o-NO₂-C₆H₄-SeCN; 2.) 30 percent H₂O₂

With copper(l) iodide; lithium aluminium tetrahydride; perchloric acid; ortho-nitrophenyl selenocyanate; tributylphosphine; hydrogen; dihydrogen peroxide; lithium; triphenylphosphine; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane;
DOI:10.1016/0040-4039(90)80114-2

Reference yield:

: 130265-30-4
(S)-1-(2,5-Dimethyl-phenyl)-3-methyl-pentane-1,5-diol

: 130323-74-9
1,4-Dimethyl-2-((R)-3-methyl-pent-4-enyl)-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: H₂, HClO₄ / 10percent Pd/C / ethanol / 15 h / 760 Torr

2: 1.) n-Bu₃P, o-NO₂-C₆H₄-SeCN; 2.) 30 percent H₂O₂

With perchloric acid; ortho-nitrophenyl selenocyanate; tributylphosphine; hydrogen; dihydrogen peroxide; palladium on activated charcoal; In ethanol;
DOI:10.1016/0040-4039(90)80114-2