benzyl N-(1-adamantyloxycarbonyl)carbamate

Base Information

Chemical Name:benzyl N-(1-adamantyloxycarbonyl)carbamate
CAS No.:120542-14-5
Molecular Formula:C₁₉H₂₃NO₄
Molecular Weight:329.396
Hs Code.:
DSSTox Substance ID:DTXSID801172858
Nikkaji Number:J435.989E

Synonyms:DTXSID801172858;120542-14-5;1-(Phenylmethyl) 3-tricyclo[3.3.1.13,7]dec-1-yl imidodicarbonate

Suppliers and Price of benzyl N-(1-adamantyloxycarbonyl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl N-(1-adamantyloxycarbonyl)carbamate

Chemical Property:

XLogP3:4.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:329.16270821
Heavy Atom Count:24
Complexity:456

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1C2CC3CC1CC(C2)(C3)OC(=O)NC(=O)OCC4=CC=CC=C4

Technology Process of benzyl N-(1-adamantyloxycarbonyl)carbamate

There total 2 articles about benzyl N-(1-adamantyloxycarbonyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 768-95-6
1-adamanthanol

: 69032-16-2
benzyloxycarbonyl isocyanate

: 120542-14-5
C₁₉H₂₃NO₄

Guidance literature:: In dichloromethane; for 15h; Ambient temperature;
DOI:10.1055/s-1988-27780

Reference yield:

: 621-84-1
O-benzyl carbamate

: 120542-14-5
C₁₉H₂₃NO₄

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / CH₂Cl₂ / 1.) 0 deg C, 1h, 2.) r.t., 4 h, 3.) reflux, 15 h

2: 98 percent / CH₂Cl₂ / 15 h / Ambient temperature

In dichloromethane;
DOI:10.1055/s-1988-27780