2,2,5,5-tetramethyl-3-(3-nitro-4-aminobenzoyl)-3-pyrrolin-1-oxyl

Base Information

Chemical Name:2,2,5,5-tetramethyl-3-(3-nitro-4-aminobenzoyl)-3-pyrrolin-1-oxyl
CAS No.:124190-13-2
Molecular Formula:C₁₈H₂₂N₃O₆
Molecular Weight:376.389
Hs Code.:

2,2,5,5-tetramethyl-3-(3-nitro-4-<N-(methoxy-carbonyl-methyl)>aminobenzoyl)-3-pyrrolin-1-oxyl

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Chemical Property of 2,2,5,5-tetramethyl-3-(3-nitro-4-aminobenzoyl)-3-pyrrolin-1-oxyl

Chemical Property:

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Technology Process of 2,2,5,5-tetramethyl-3-(3-nitro-4-aminobenzoyl)-3-pyrrolin-1-oxyl

There total 4 articles about 2,2,5,5-tetramethyl-3-(3-nitro-4-aminobenzoyl)-3-pyrrolin-1-oxyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 124189-92-0
2,2,5,5-tetramethyl-3-(3-nitro-4-fluorobenzoyl)-3-pyrrolin-1-oxyl

: 124190-13-2
2,2,5,5-tetramethyl-3-(3-nitro-4-aminobenzoyl)-3-pyrrolin-1-oxyl

Guidance literature:: With potassium carbonate; In ethanol; for 3h; Heating;

Reference yield:

: 71051-83-7
3-formyl-2,2,5,5-tetramethyl-pyrroline-1-oxyl

: 124190-13-2
2,2,5,5-tetramethyl-3-(3-nitro-4-aminobenzoyl)-3-pyrrolin-1-oxyl

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) CdCl₂; 2.) MnO₂ / 1.) ether, room temperature, 6h; 2.) CCl₄, reflux, 6h

2: 84 percent / conc. H₂SO₄, 67percent HNO₃ / H₂O / 0.5 h / 0 °C

3: 72 percent / K₂CO₃ / aq. ethanol / 3 h / Heating

With manganese(IV) oxide; sulfuric acid; nitric acid; potassium carbonate; cadmium(II) chloride; In ethanol; water;

Reference yield:

: 352-13-6
4-flourophenylmagnesium bromide

: 124190-13-2
2,2,5,5-tetramethyl-3-(3-nitro-4-aminobenzoyl)-3-pyrrolin-1-oxyl

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) CdCl₂; 2.) MnO₂ / 1.) ether, room temperature, 6h; 2.) CCl₄, reflux, 6h

2: 84 percent / conc. H₂SO₄, 67percent HNO₃ / H₂O / 0.5 h / 0 °C

3: 72 percent / K₂CO₃ / aq. ethanol / 3 h / Heating

With manganese(IV) oxide; sulfuric acid; nitric acid; potassium carbonate; cadmium(II) chloride; In ethanol; water;