N-[(2S,3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-5-((2S,4aR,6S,7R,8S,8aS)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-2-hydroxy-tetrahydro-pyran-3-yl]-2,2,2-trichloro-acetamide

Base Information

Chemical Name:N-[(2S,3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-5-((2S,4aR,6S,7R,8S,8aS)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-2-hydroxy-tetrahydro-pyran-3-yl]-2,2,2-trichloro-acetamide
CAS No.:503831-00-3
Molecular Formula:C₄₉H₅₀Cl₃NO₁₁
Molecular Weight:935.295
Hs Code.:

N-[(2S,3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-5-((2S,4aR,6S,7R,8S,8aS)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-2-hydroxy-tetrahydro-pyran-3-yl]-2,2,2-trichloro-acetamide

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Suppliers and Price of N-[(2S,3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-5-((2S,4aR,6S,7R,8S,8aS)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-2-hydroxy-tetrahydro-pyran-3-yl]-2,2,2-trichloro-acetamide

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Chemical Property of N-[(2S,3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-5-((2S,4aR,6S,7R,8S,8aS)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-2-hydroxy-tetrahydro-pyran-3-yl]-2,2,2-trichloro-acetamide

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Technology Process of N-[(2S,3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-5-((2S,4aR,6S,7R,8S,8aS)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-2-hydroxy-tetrahydro-pyran-3-yl]-2,2,2-trichloro-acetamide

There total 14 articles about N-[(2S,3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-5-((2S,4aR,6S,7R,8S,8aS)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-2-hydroxy-tetrahydro-pyran-3-yl]-2,2,2-trichloro-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 503831-00-3
N-[(2S,3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-5-((2S,4aR,6S,7R,8S,8aS)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-2-hydroxy-tetrahydro-pyran-3-yl]-2,2,2-trichloro-acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: pTsOH / acetonitrile

2: NaH / dimethylformamide

3: Zn; AcOH / CH₂Cl₂

4: 87 percent / pyridine

5: n-Bu₄NF; AcOH / tetrahydrofuran

With pyridine; tetrabutyl ammonium fluoride; sodium hydride; toluene-4-sulfonic acid; acetic acid; zinc; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(02)01947-0

Reference yield:

: 3068-32-4
1-bromo-1-deoxy-2,3,4,6-tetra-O-acetyl-a-D-galactopyranoside

: 503831-00-3
N-[(2S,3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-5-((2S,4aR,6S,7R,8S,8aS)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-2-hydroxy-tetrahydro-pyran-3-yl]-2,2,2-trichloro-acetamide

Guidance literature:: Multi-step reaction with 7 steps

1: 80 percent / AgOTf

2: NaOMe / methanol

3: pTsOH / acetonitrile

4: NaH / dimethylformamide

5: Zn; AcOH / CH₂Cl₂

6: 87 percent / pyridine

7: n-Bu₄NF; AcOH / tetrahydrofuran

With pyridine; tetrabutyl ammonium fluoride; sodium methylate; silver trifluoromethanesulfonate; sodium hydride; toluene-4-sulfonic acid; acetic acid; zinc; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(02)01947-0