(6R,6'R)-3,3'-bis-acetoxymethyl-7,7'-bis-(3,5-di-tert-butyl-4-hydroxy-benzylideneamino)-8,8'-dioxo-(6rH,7tH,6'r'H,7't'H)-[7,7']bi[5-thia-1-aza-bicyclo[4.2.0]octyl]-2,2'-diene-2,2'-dicarboxylic acid dibenzhydryl ester

Base Information

• Chemical Name: (6R,6'R)-3,3'-bis-acetoxymethyl-7,7'-bis-(3,5-di-tert-butyl-4-hydroxy-benzylideneamino)-8,8'-dioxo-(6rH,7tH,6'r'H,7't'H)-[7,7']bi[5-thia-1-aza-bicyclo[4.2.0]octyl]-2,2'-diene-2,2'-dicarboxylic acid dibenzhydryl ester
• CAS No.: 61309-61-3
• Molecular Formula: C₇₆H₈₂N₄O₁₂S₂
• Molecular Weight: 1307.64
• Mol file: 61309-61-3.mol

Synonyms:

Chemical Property of (6R,6'R)-3,3'-bis-acetoxymethyl-7,7'-bis-(3,5-di-tert-butyl-4-hydroxy-benzylideneamino)-8,8'-dioxo-(6rH,7tH,6'r'H,7't'H)-[7,7']bi[5-thia-1-aza-bicyclo[4.2.0]octyl]-2,2'-diene-2,2'-dicarboxylic acid dibenzhydryl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (6R,6'R)-3,3'-bis-acetoxymethyl-7,7'-bis-(3,5-di-tert-butyl-4-hydroxy-benzylideneamino)-8,8'-dioxo-(6rH,7tH,6'r'H,7't'H)-[7,7']bi[5-thia-1-aza-bicyclo[4.2.0]octyl]-2,2'-diene-2,2'-dicarboxylic acid dibenzhydryl ester

There total 1 articles about (6R,6'R)-3,3'-bis-acetoxymethyl-7,7'-bis-(3,5-di-tert-butyl-4-hydroxy-benzylideneamino)-8,8'-dioxo-(6rH,7tH,6'r'H,7't'H)-[7,7']bi[5-thia-1-aza-bicyclo[4.2.0]octyl]-2,2'-diene-2,2'-dicarboxylic acid dibenzhydryl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-3-acetoxymethyl-7-(3,5-di-tert-butyl-4-oxo-cyclohexa-2,5-dienylidenemethylimino)-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzhydryl ester (57270-11-8) → (6R,6'R)-3,3'-bis-acetoxymethyl-7,7'-bis-(3,5-di-tert-butyl-4-hydroxy-benzylideneamino)-8,8'-dioxo-(6rH,7tH,6'r'H,7't'H)-[7,7']bi[5-thia-1-aza-bicyclo[4.2.0]octyl]-2,2'-diene-2,2'-dicarboxylic acid dibenzhydryl ester (61309-61-3)

Guidance literature:

With phosphorous acid trimethyl ester; In benzene; Ambient temperature;

DOI:10.1016/S0040-4039(00)93790-0

Reference yield:

(6R,6'R)-3,3'-bis-acetoxymethyl-7,7'-bis-(3,5-di-tert-butyl-4-hydroxy-benzylideneamino)-8,8'-dioxo-(6rH,7tH,6'r'H,7't'H)-[7,7']bi[5-thia-1-aza-bicyclo[4.2.0]octyl]-2,2'-diene-2,2'-dicarboxylic acid dibenzhydryl ester (61309-61-3) → (6R,6'R)-3,3'-bis-acetoxymethyl-7,7'-diamino-8,8'-dioxo-(6rH,7tH,6'r'H,7't'H)-[7,7']bi[5-thia-1-aza-bicyclo[4.2.0]octyl]-2,2'-diene-2,2'-dicarboxylic acid dibenzhydryl ester (61253-48-3)

Guidance literature:

With toluene-4-sulfonic acid; (2,4-dinitro-phenyl)-hydrazine; In ethanol;

DOI:10.1016/S0040-4039(00)93790-0

Reference yield:

(6R,6'R)-3,3'-bis-acetoxymethyl-7,7'-bis-(3,5-di-tert-butyl-4-hydroxy-benzylideneamino)-8,8'-dioxo-(6rH,7tH,6'r'H,7't'H)-[7,7']bi[5-thia-1-aza-bicyclo[4.2.0]octyl]-2,2'-diene-2,2'-dicarboxylic acid dibenzhydryl ester (61309-61-3) + acetone (67-64-1) → (7R,7''R)-3,3''-bis-acetoxymethyl-2',2'-dimethyl-8,8''-dioxo-(6tH,7rN,6''t'H,7''r'N)-dispiro[5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-7,4'-imidazolidine-5',7''-(5-thia-1-aza-bicyclo[4.2.0]oct-2-ene)]-2,2''-dicarboxylic acid dibenzhydryl ester (61253-47-2)

Guidance literature:

With hydrogenchloride; In acetone; Ambient temperature;

DOI:10.1016/S0040-4039(00)93790-0

upstream raw materials:

(R)-3-acetoxymethyl-7-(3,5-di-tert-butyl-4-oxo-cyclohexa-2,5-dienylidenemethylimino)-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzhydryl ester

Downstream raw materials:

(6R,6'R)-3,3'-bis-acetoxymethyl-7,7'-diamino-8,8'-dioxo-(6rH,7tH,6'r'H,7't'H)-[7,7']bi[5-thia-1-aza-bicyclo[4.2.0]octyl]-2,2'-diene-2,2'-dicarboxylic acid dibenzhydryl ester

(7R,7''R)-3,3''-bis-acetoxymethyl-2',2'-dimethyl-8,8''-dioxo-(6tH,7rN,6''t'H,7''r'N)-dispiro[5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-7,4'-imidazolidine-5',7''-(5-thia-1-aza-bicyclo[4.2.0]oct-2-ene)]-2,2''-dicarboxylic acid dibenzhydryl ester