all-trans-dichlorobis[(2-hydroxyethyl)isocyanide]bis(triphenylphosphane)ruthenium

Base Information

Chemical Name:all-trans-dichlorobis[(2-hydroxyethyl)isocyanide]bis(triphenylphosphane)ruthenium
CAS No.:97385-57-4
Molecular Formula:C₄₂H₄₀Cl₂N₂O₂P₂Ru
Molecular Weight:838.715
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Chemical Property of all-trans-dichlorobis[(2-hydroxyethyl)isocyanide]bis(triphenylphosphane)ruthenium

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Technology Process of all-trans-dichlorobis[(2-hydroxyethyl)isocyanide]bis(triphenylphosphane)ruthenium

There total 1 articles about all-trans-dichlorobis[(2-hydroxyethyl)isocyanide]bis(triphenylphosphane)ruthenium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 15529-49-4,41756-81-4
tris(triphenylphosphine)ruthenium(II) chloride

: 32835-59-9
(2-Hydroxyethyl)isocyanid

: 97385-57-4
all-trans-dichlorobis[(2-hydroxyethyl)isocyanide]bis(triphenylphosphane)ruthenium

Guidance literature:: In acetone; dropwise addn. of the isocyanide in acetone to a soln. of RuCl2(PPh3)3 in acetone under N2, immediate colour change to light yellow; concg. to 1/3 of the vol. (after 2 h), layering with Et2O, pptn. (-20°C), washing (ether, 3 times), drying (high vac.), recrystn. (acetone/ether); elem. anal.;