(2,4,6-trimethylphenyl)tribromogermane

Base Information

Chemical Name:(2,4,6-trimethylphenyl)tribromogermane
CAS No.:114806-83-6
Molecular Formula:C₉H₁₁Br₃Ge
Molecular Weight:431.488
Hs Code.:

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Chemical Property of (2,4,6-trimethylphenyl)tribromogermane

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Technology Process of (2,4,6-trimethylphenyl)tribromogermane

There total 1 articles about (2,4,6-trimethylphenyl)tribromogermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: germanium(II) chloride dioxane

: 576-83-0
2,4,6-trimethylphenyl bromide

: 114806-82-5
(2,4,6-trimethylphenyl)trichlorogermane

: 114806-83-6
(2,4,6-trimethylphenyl)tribromogermane

Guidance literature:: aluminium trichloride; In further solvent(s); byproducts: dioxane; N2-atmosphere; bromomesitylene as solvent, heating at 80°C for 4 d; cooling, filtration, evapn. off of dioxane, distillation off of bromotoluene (43°C, 0.05 mbar), not sepd.; mass-spectroscopy, 80% altogether yield;
DOI:10.1021/om990349z

Reference yield: 76.0%

: 16853-85-3
lithium aluminium tetrahydride

: 114806-82-5
(2,4,6-trimethylphenyl)trichlorogermane

: 114806-83-6
(2,4,6-trimethylphenyl)tribromogermane

: 72876-20-1
2,4,6-trimethylphenylgermanium trihydride

Guidance literature:: In diethyl ether; N2-atmosphere; addn. of soln. of Ge-compounds (chloride:bromide 2:1 mixt.) to suspension of LiAlH4, refluxing for 2 h; evapn., extn. (pentane), distillation (85°C, 4 mbar); elem. anal.;
DOI:10.1021/om990349z