N-benzyl-N-(6,7-dimethoxy-4-methyl-3,4-dihydronaphthalen-2-yl)benzamide

Base Information

Chemical Name:N-benzyl-N-(6,7-dimethoxy-4-methyl-3,4-dihydronaphthalen-2-yl)benzamide
CAS No.:1315171-97-1
Molecular Formula:C₂₇H₂₇NO₃
Molecular Weight:413.516
Hs Code.:

Synonyms:

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Chemical Property of N-benzyl-N-(6,7-dimethoxy-4-methyl-3,4-dihydronaphthalen-2-yl)benzamide

Chemical Property:

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Technology Process of N-benzyl-N-(6,7-dimethoxy-4-methyl-3,4-dihydronaphthalen-2-yl)benzamide

There total 6 articles about N-benzyl-N-(6,7-dimethoxy-4-methyl-3,4-dihydronaphthalen-2-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1315171-93-7
3-(4,5-dimethoxy-2-methoxycarbonylmethylphenyl)butyric acid methyl ester

: 1315171-97-1
N-benzyl-N-(6,7-dimethoxy-4-methyl-3,4-dihydronaphthalen-2-yl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butylate / diethyl ether / 0.75 h / 20 °C / Inert atmosphere

1.2: 125 °C / Inert atmosphere

2.1: toluene / Reflux; Inert atmosphere

3.1: triethylamine / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice

With potassium tert-butylate; triethylamine; In diethyl ether; dichloromethane; toluene; 1.1: Dieckmann condensation;
DOI:10.1021/jm200334c

Reference yield:

: 1315171-95-9
6,7-dimethoxy-4-methyl-3,4-dihydro-1H-naphthalen-2-one

: 1315171-97-1
N-benzyl-N-(6,7-dimethoxy-4-methyl-3,4-dihydronaphthalen-2-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / Reflux; Inert atmosphere

2: triethylamine / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice

With triethylamine; In dichloromethane; toluene;
DOI:10.1021/jm200334c

Reference yield:

: 93-40-3
(3,4-Dimethoxyphenyl)acetic acid

: 1315171-97-1
N-benzyl-N-(6,7-dimethoxy-4-methyl-3,4-dihydronaphthalen-2-yl)benzamide

Guidance literature:: Multi-step reaction with 7 steps

1.1: Iodine monochloride; acetic acid / dichloromethane / Inert atmosphere

2.1: Amberlyst / Inert atmosphere

3.1: bis-triphenylphosphine-palladium(II) chloride; triethylamine / acetonitrile / 96 h / Inert atmosphere; Reflux

4.1: hydrogen / ethanol / 3102.97 Torr

5.1: potassium tert-butylate / diethyl ether / 0.75 h / 20 °C / Inert atmosphere

5.2: 125 °C / Inert atmosphere

6.1: toluene / Reflux; Inert atmosphere

7.1: triethylamine / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice

With bis-triphenylphosphine-palladium(II) chloride; potassium tert-butylate; hydrogen; Iodine monochloride; acetic acid; triethylamine; In diethyl ether; ethanol; dichloromethane; toluene; acetonitrile; 3.1: Heck reaction / 5.1: Dieckmann condensation;
DOI:10.1021/jm200334c