trans-[Fe(CO)3(PPh₃)(Sb₂Ph₄)]

Base Information

• Chemical Name: trans-[Fe(CO)3(PPh₃)(Sb₂Ph₄)]
• CAS No.: 857498-21-6
• Molecular Formula: C₄₅H₃₅FeO₃PSb₂
• Molecular Weight: 954.092
• Mol file: 857498-21-6.mol

Synonyms:

Chemical Property of trans-[Fe(CO)3(PPh₃)(Sb₂Ph₄)]

Chemical Property:

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Technology Process of trans-[Fe(CO)3(PPh₃)(Sb₂Ph₄)]

There total 1 articles about trans-[Fe(CO)3(PPh₃)(Sb₂Ph₄)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

K2[Fe(CO)3(PPh3)] (80612-34-6) + diphenylantimony(III) chloride (2629-47-2) → trans-[Fe(CO)3(PPh3)(Sb2Ph4)] (857498-21-6)

Guidance literature:

In tetrahydrofuran; byproducts: KCl; under Ar; soln. of K2Fe(CO)3(PPh3) (0.259 mmol) and Ph2SbCl (0.518 mmol)in THF stirred for 2 h; evapd. under vac.; repeatedly recrystd. from CH2Cl2/n-hexane; dried under vac.; elem. anal.;

DOI:10.1002/ejic.200400683

upstream raw materials:

K₂[Fe(CO)3(PPh₃)]

diphenylantimony(III) chloride